(1S,2R,3S,4S)-4-isopropenyl-3-{[(p-methoxyphenyl)methoxy]methyl}-2-methylcyclopentanol

Base Information

Chemical Name:(1S,2R,3S,4S)-4-isopropenyl-3-{[(p-methoxyphenyl)methoxy]methyl}-2-methylcyclopentanol
CAS No.:1621399-33-4
Molecular Formula:C₁₈H₂₆O₃
Molecular Weight:290.403
Hs Code.:

Synonyms:(1S,2R,3S,4S)-4-isopropenyl-3-{[(p-methoxyphenyl)methoxy]methyl}-2-methylcyclopentanol

Suppliers and Price of (1S,2R,3S,4S)-4-isopropenyl-3-{[(p-methoxyphenyl)methoxy]methyl}-2-methylcyclopentanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,3S,4S)-4-isopropenyl-3-{[(p-methoxyphenyl)methoxy]methyl}-2-methylcyclopentanol

Chemical Property:

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Technology Process of (1S,2R,3S,4S)-4-isopropenyl-3-{[(p-methoxyphenyl)methoxy]methyl}-2-methylcyclopentanol

There total 3 articles about (1S,2R,3S,4S)-4-isopropenyl-3-{[(p-methoxyphenyl)methoxy]methyl}-2-methylcyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[(1S,2S,3R,4S)-2-{[(p-methoxyphenyl)methoxy]methyl}-3-methyl-4-(tetrahydro-2H-pyran-2-yloxy)cyclopentyl]prop-1-ene

: 1621399-33-4
(1S,2R,3S,4S)-4-isopropenyl-3-{[(p-methoxyphenyl)methoxy]methyl}-2-methylcyclopentanol

Guidance literature:: With pyridinium p-toluenesulfonate; In methanol; for 15h;
DOI:10.1055/s-0033-1338573

Reference yield:

: 881425-05-4
[(1S,2R,3S,5S)-2-methyl-5-(prop-1-en-2-yl)-3-(tetrahydro-2H-pyran-2-yloxy)cyclopentyl]methanol

: 1621399-33-4
(1S,2R,3S,4S)-4-isopropenyl-3-{[(p-methoxyphenyl)methoxy]methyl}-2-methylcyclopentanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

1.2: 2.67 h

2.1: pyridinium p-toluenesulfonate / methanol / 15 h

With pyridinium p-toluenesulfonate; sodium hydride; In methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1055/s-0033-1338573

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1621399-33-4
(1S,2R,3S,4S)-4-isopropenyl-3-{[(p-methoxyphenyl)methoxy]methyl}-2-methylcyclopentanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

1.2: 2.67 h

2.1: pyridinium p-toluenesulfonate / methanol / 15 h

With pyridinium p-toluenesulfonate; sodium hydride; In methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1055/s-0033-1338573