C₁₁H₁₃Cl₂NO

Base Information

Chemical Name:C₁₁H₁₃Cl₂NO
CAS No.:1004551-77-2
Molecular Formula:C₁₁H₁₃Cl₂NO
Molecular Weight:246.136
Hs Code.:

C<sub>11</sub>H<sub>13</sub>Cl<sub>2</sub>NO

Synonyms:C₁₁H₁₃Cl₂NO

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Chemical Property of C₁₁H₁₃Cl₂NO

Chemical Property:

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Technology Process of C₁₁H₁₃Cl₂NO

There total 2 articles about C₁₁H₁₃Cl₂NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(3,4-dichlorophenyl)-2-hydroxymethyl-cyclopropanecarbonitrile

: 1004551-77-2
C₁₁H₁₃Cl₂NO

Guidance literature:: 1-(3,4-dichlorophenyl)-2-hydroxymethyl-cyclopropanecarbonitrile; With dimethylsulfide borane complex; In tetrahydrofuran; at 40 ℃; for 6.5h; Inert atmosphere; Industry scale;

With hydrogenchloride; water; In tetrahydrofuran; at 40 ℃; for 1h; Industry scale;

With ammonium hydroxide; In tetrahydrofuran; water; Industry scale;

Reference yield:

: 3218-49-3
3,4-dichloro-benzeneacetonitrile

: 1004551-77-2
C₁₁H₁₃Cl₂NO

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / -15 - -5 °C / Inert atmosphere; Industry scale

2.1: dimethylsulfide borane complex / tetrahydrofuran / 6.5 h / 40 °C / Inert atmosphere; Industry scale

2.2: 1 h / 40 °C / Industry scale

2.3: Industry scale

With dimethylsulfide borane complex; sodium hexamethyldisilazane; In tetrahydrofuran;

Reference yield:

: 1004551-77-2
C₁₁H₁₃Cl₂NO

: 410074-74-7
Amitifadine hydrochloride

Guidance literature:: C₁₁H₁₃Cl₂NO; With thionyl chloride; In Isopropyl acetate; at 20 ℃; Inert atmosphere; Industry scale;

With sodium hydroxide; In Isopropyl acetate; at 20 - 30 ℃; for 2h; pH=8.5 - 9;

With hydrogenchloride; In Isopropyl acetate; water; isopropyl alcohol;