C₁₇H₂₆O₃

Base Information

Chemical Name:C₁₇H₂₆O₃
CAS No.:1418183-68-2
Molecular Formula:C₁₇H₂₆O₃
Molecular Weight:278.392
Hs Code.:

C<sub>17</sub>H<sub>26</sub>O<sub>3</sub>

Synonyms:C₁₇H₂₆O₃

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Chemical Property of C₁₇H₂₆O₃

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Technology Process of C₁₇H₂₆O₃

There total 8 articles about C₁₇H₂₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1418183-67-1
(R)-2-ethylhexyl (E)-3-[3-(benzyloxy)phenyl]acrylate

: 1418183-68-2
C₁₇H₂₆O₃

Guidance literature:: With 10% Pd/C; hydrogen; In tetrahydrofuran; at 20 ℃; for 7h; enantioselective reaction;
DOI:10.1055/s-0032-1316776

Reference yield:

: 142-62-1
hexanoic acid

: 1418183-68-2
C₁₇H₂₆O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; dmap / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

2.1: titanium tetrachloride; sparteine / dichloromethane / 0.33 h / Inert atmosphere; Cooling with ice

2.2: -78 °C / Inert atmosphere; Cooling with acetone-dry ice

2.3: 1 h / 0 °C / Inert atmosphere

3.1: dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 8 h / 110 °C / Inert atmosphere

5.1: sodium tetrahydroborate / methanol / 3 h / 20 °C / Cooling with ice

6.1: 2-methyl-6-nitrobenzoic anhydride; dmap; triethylamine / toluene / 3 h / 20 °C / Molecular sieve

7.1: hydrogen; 10% Pd/C / tetrahydrofuran / 7 h / 20 °C

With dmap; sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); 10% Pd/C; 2-methyl-6-nitrobenzoic anhydride; hydrogen; tri-n-butyl-tin hydride; titanium tetrachloride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; sparteine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1055/s-0032-1316776

Reference yield:

: 1418183-62-6
(S)-3-hexanoyl-4-phenyloxazolidin-2-one

: 1418183-68-2
C₁₇H₂₆O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: titanium tetrachloride; sparteine / dichloromethane / 0.33 h / Inert atmosphere; Cooling with ice

1.2: -78 °C / Inert atmosphere; Cooling with acetone-dry ice

1.3: 1 h / 0 °C / Inert atmosphere

2.1: dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 8 h / 110 °C / Inert atmosphere

4.1: sodium tetrahydroborate / methanol / 3 h / 20 °C / Cooling with ice

5.1: 2-methyl-6-nitrobenzoic anhydride; dmap; triethylamine / toluene / 3 h / 20 °C / Molecular sieve

6.1: hydrogen; 10% Pd/C / tetrahydrofuran / 7 h / 20 °C

With dmap; sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); 10% Pd/C; 2-methyl-6-nitrobenzoic anhydride; hydrogen; tri-n-butyl-tin hydride; titanium tetrachloride; triethylamine; sparteine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1055/s-0032-1316776