(S)-α-[2,2-bis(phenylsulfonyl)ethyl]-α-(tert-butoxycarbonylamino)-benzeneacetaldehyde

Base Information

Chemical Name:(S)-α-[2,2-bis(phenylsulfonyl)ethyl]-α-(tert-butoxycarbonylamino)-benzeneacetaldehyde
CAS No.:1257438-06-4
Molecular Formula:C₂₇H₂₉NO₇S₂
Molecular Weight:543.662
Hs Code.:

Synonyms:(S)-α-[2,2-bis(phenylsulfonyl)ethyl]-α-(tert-butoxycarbonylamino)-benzeneacetaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-α-[2,2-bis(phenylsulfonyl)ethyl]-α-(tert-butoxycarbonylamino)-benzeneacetaldehyde

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Technology Process of (S)-α-[2,2-bis(phenylsulfonyl)ethyl]-α-(tert-butoxycarbonylamino)-benzeneacetaldehyde

There total 2 articles about (S)-α-[2,2-bis(phenylsulfonyl)ethyl]-α-(tert-butoxycarbonylamino)-benzeneacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 39082-53-6
1,1-bis(phenylsulfonyl)ethylene

: 140196-38-9
1,1-dimethyl (2-oxo-1-phenylethyl)carbamate

: 1257438-06-4
(S)-α-[2,2-bis(phenylsulfonyl)ethyl]-α-(tert-butoxycarbonylamino)-benzeneacetaldehyde

Guidance literature:: With (S,S)-N-Tf-11,12-diamino-9,10-dihydro-9,10-ethanoanthracene; 2,6-Dihydroxybenzoic acid; In toluene; at -20 ℃; for 12h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ja107897t

Reference yield:

: 39082-53-6
1,1-bis(phenylsulfonyl)ethylene

: 140196-38-9
1,1-dimethyl (2-oxo-1-phenylethyl)carbamate

: 1257438-06-4
(S)-α-[2,2-bis(phenylsulfonyl)ethyl]-α-(tert-butoxycarbonylamino)-benzeneacetaldehyde

: (R)-α-[2,2-bis(phenylsulfonyl)ethyl]-α-(tert-butoxycarbonylamino)-benzeneacetaldehyde

Guidance literature:: With (S,S)-N-Tf-11,12-diamino-9,10-dihydro-9,10-ethanoanthracene; trifluoroacetic acid; In toluene; at 20 ℃; for 3h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ja107897t