C₃₂H₃₈O₅

Base Information

Chemical Name:C₃₂H₃₈O₅
CAS No.:1264756-79-7
Molecular Formula:C₃₂H₃₈O₅
Molecular Weight:502.651
Hs Code.:

C<sub>32</sub>H<sub>38</sub>O<sub>5</sub>

Synonyms:C₃₂H₃₈O₅

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Chemical Property of C₃₂H₃₈O₅

Chemical Property:

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Technology Process of C₃₂H₃₈O₅

There total 14 articles about C₃₂H₃₈O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1264756-65-1
C₂₄H₃₀O₄

: 824-94-2
p-methoxybenzyl chloride

: 1264756-79-7
C₃₂H₃₈O₅

Guidance literature:: With potassium tert-butylate; tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: 1264756-61-7
C₂₈H₃₄O₅

: 1264756-79-7
C₃₂H₃₈O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C

1.2: 20 °C

2.1: diisobutylaluminium hydride / dichloromethane / -78 °C

3.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

4.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

6.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

7.1: potassium tert-butylate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hypochlorite; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl (2R,3R)-tartrate; potassium tert-butylate; water; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 1.1: Swern oxidation / 1.2: Wittig reaction / 3.1: Sharpless asymmetric epoxidation / 5.1: Wittig reaction;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: 1264756-62-8
C₃₃H₄₀O₆

: 1264756-79-7
C₃₂H₃₈O₅

Guidance literature:: Multi-step reaction with 6 steps

1: diisobutylaluminium hydride / dichloromethane / -78 °C

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

3: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

4: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

5: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

6: potassium tert-butylate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl (2R,3R)-tartrate; potassium tert-butylate; water; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 2: Sharpless asymmetric epoxidation / 4: Wittig reaction;
DOI:10.1016/j.tetlet.2010.11.127