(Z)-N-(3-(2-acetamido-2-oxo-1-(trityloxyimino)ethyl)-1,2,4-thiadiazol-5-yl)benzamide

Base Information

• Chemical Name: (Z)-N-(3-(2-acetamido-2-oxo-1-(trityloxyimino)ethyl)-1,2,4-thiadiazol-5-yl)benzamide
• CAS No.: 1283593-52-1
• Molecular Formula: C₃₂H₂₅N₅O₄S
• Molecular Weight: 575.648

Synonyms:(Z)-N-(3-(2-acetamido-2-oxo-1-(trityloxyimino)ethyl)-1,2,4-thiadiazol-5-yl)benzamide

Chemical Property of (Z)-N-(3-(2-acetamido-2-oxo-1-(trityloxyimino)ethyl)-1,2,4-thiadiazol-5-yl)benzamide

Chemical Property:

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Technology Process of (Z)-N-(3-(2-acetamido-2-oxo-1-(trityloxyimino)ethyl)-1,2,4-thiadiazol-5-yl)benzamide

There total 1 articles about (Z)-N-(3-(2-acetamido-2-oxo-1-(trityloxyimino)ethyl)-1,2,4-thiadiazol-5-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

N-(3-(2-acetamido-2-oxoethyl)-1,2,4-thiadiazol-5-yl)benzamide (1264195-43-8) + trityl chloride (76-83-5) → (Z)-N-(3-(2-acetamido-2-oxo-1-(trityloxyimino)ethyl)-1,2,4-thiadiazol-5-yl)benzamide (1283593-52-1)

Guidance literature:

N-(3-(2-acetamido-2-oxoethyl)-1,2,4-thiadiazol-5-yl)benzamide; With hydrogenchloride; i-propyl nitrite; In tetrahydrofuran; water; at 25 ℃; for 5h;

trityl chloride; With triethylamine; In tetrahydrofuran; water; at 25 ℃; for 2.5h; pH=10; stereoselective reaction;

DOI:10.1021/op100323b

Reference yield: 48.0%

(Z)-N-(3-(2-acetamido-2-oxo-1-(trityloxyimino)ethyl)-1,2,4-thiadiazol-5-yl)benzamide (1283593-52-1) → (Z)-2-(5-amino-1,2,4-thiadiazol-3-yl)-2-(triphenylmethoxyimino)acetic acid

Guidance literature:

With water; sodium hydroxide; at 100 ℃; for 8h;

DOI:10.1021/op100323b

upstream raw materials:

N-(3-(2-acetamido-2-oxoethyl)-1,2,4-thiadiazol-5-yl)benzamide

trityl chloride

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