1-(3-Chloro-4-fluoro-phenyl)-2-(2-chloro-4-nitro-phenylsulfanyl)-ethanone

Base Information

Chemical Name:1-(3-Chloro-4-fluoro-phenyl)-2-(2-chloro-4-nitro-phenylsulfanyl)-ethanone
CAS No.:203251-41-6
Molecular Formula:C₁₄H₈Cl₂FNO₃S
Molecular Weight:360.193
Hs Code.:

Synonyms:1-(3-Chloro-4-fluoro-phenyl)-2-(2-chloro-4-nitro-phenylsulfanyl)-ethanone

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Chemical Property of 1-(3-Chloro-4-fluoro-phenyl)-2-(2-chloro-4-nitro-phenylsulfanyl)-ethanone

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Technology Process of 1-(3-Chloro-4-fluoro-phenyl)-2-(2-chloro-4-nitro-phenylsulfanyl)-ethanone

There total 1 articles about 1-(3-Chloro-4-fluoro-phenyl)-2-(2-chloro-4-nitro-phenylsulfanyl)-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 36776-29-1
2-chloro-4-nitro-thiophenol

: 2-chloro-1-(3-chloro-4-fluorophenyl)-ethanone

: 203251-41-6
1-(3-Chloro-4-fluoro-phenyl)-2-(2-chloro-4-nitro-phenylsulfanyl)-ethanone

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In water; acetone; for 1h; Ambient temperature;
DOI:10.1002/jhet.5570340603

Reference yield: 58.0%

: 203251-41-6
1-(3-Chloro-4-fluoro-phenyl)-2-(2-chloro-4-nitro-phenylsulfanyl)-ethanone

: 203251-44-9
1-(3-Chloro-4-fluoro-phenyl)-2-(2-chloro-4-nitro-benzenesulfonyl)-ethanone

Guidance literature:: With dihydrogen peroxide; In acetic acid; at 55 ℃; for 8h;
DOI:10.1002/jhet.5570340603

Reference yield:

: 203251-41-6
1-(3-Chloro-4-fluoro-phenyl)-2-(2-chloro-4-nitro-phenylsulfanyl)-ethanone

: 3-[3-(2-benzoxazolyl)benzyl]-2-(3-chloro-4-fluorophenyl)-7-nitro-1,4-benzoxathiin 4,4-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / 30percent aq. H₂O₂ / acetic acid / 8 h / 55 °C

2: 68 percent / K₂CO₃, triethylbenzylammonium chloride / dimethylformamide / 10 h / 60 °C

With N-benzyl-N,N,N-triethylammonium chloride; dihydrogen peroxide; potassium carbonate; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570340603