2,3-μ-N-benzylcarbamoyl-1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-μ-hydrido-triangulo-triosmium

Base Information

Chemical Name:2,3-μ-N-benzylcarbamoyl-1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-μ-hydrido-triangulo-triosmium
CAS No.:69198-59-0
Molecular Formula:C₁₈H₉NO₁₁Os₃
Molecular Weight:985.87
Hs Code.:

Synonyms:2,3-μ-N-benzylcarbamoyl-1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-μ-hydrido-triangulo-triosmium

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Chemical Property of 2,3-μ-N-benzylcarbamoyl-1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-μ-hydrido-triangulo-triosmium

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Technology Process of 2,3-μ-N-benzylcarbamoyl-1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-μ-hydrido-triangulo-triosmium

There total 2 articles about 2,3-μ-N-benzylcarbamoyl-1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-μ-hydrido-triangulo-triosmium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 15696-40-9
dodecacarbonyl triosmium

: 100-46-9
benzylamine

: 2,3-μ-benzyl-1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-μ-hydrido-triangulo-triosmium

: 69198-59-0
2,3-μ-N-benzylcarbamoyl-1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-μ-hydrido-triangulo-triosmium

Guidance literature:: With carbon monoxide; In octane; excess benzylamine, refluxing for 3.5-7 h with bubbling CO through soln.; evapn. (reduced pressure), TLC (SiO2, <=7% CHCl3 in light petroleum); elem. anal.; yield of benzylamido-complex increasing with reaction time;

Reference yield:

: [Os₃(CO)10(cyclooctene)2]

: 100-46-9
benzylamine

: 2,3-μ-benzyl-1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-μ-hydrido-triangulo-triosmium

: 69198-59-0
2,3-μ-N-benzylcarbamoyl-1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-μ-hydrido-triangulo-triosmium

Guidance literature:: With cyclo-octene; In cyclohexane; absence of air and moisture; 60-70°C, 2 h; solvent removal (reduced pressure), chromy. (silica);