5,6-dideoxy-1,2-O-isopropylidene-5-C-<(methoxy)phenylphosphinyl>-3-O-methyl-α-D-glucofuranose

Base Information

• Chemical Name: 5,6-dideoxy-1,2-O-isopropylidene-5-C-<(methoxy)phenylphosphinyl>-3-O-methyl-α-D-glucofuranose
• CAS No.: 70632-56-3
• Molecular Formula: C₁₇H₂₅O₆P
• Molecular Weight: 356.356

Synonyms:5,6-dideoxy-1,2-O-isopropylidene-5-C-<(methoxy)phenylphosphinyl>-3-O-methyl-α-D-glucofuranose

Chemical Property of 5,6-dideoxy-1,2-O-isopropylidene-5-C-<(methoxy)phenylphosphinyl>-3-O-methyl-α-D-glucofuranose

Chemical Property:

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Technology Process of 5,6-dideoxy-1,2-O-isopropylidene-5-C-<(methoxy)phenylphosphinyl>-3-O-methyl-α-D-glucofuranose

There total 12 articles about 5,6-dideoxy-1,2-O-isopropylidene-5-C-<(methoxy)phenylphosphinyl>-3-O-methyl-α-D-glucofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(5-RS)-5,6-anhydro-3-O-benzyl-5-C-<(ethoxy)phenylphosphinyl>-1,2-O-isopropylidene-α-D-xylo-hexafuranose (76707-49-8,83212-98-0,83212-99-1) → (5RS)-3-O-benzyl-5,6-dideoxy-5-C-<(ethoxy)phenylphosphinyl>-1,2-O-isopropylidene-α-D-xylo-hexofuranose (66034-26-2,70632-56-3,130930-04-0,134356-03-9,134356-04-0)

Guidance literature:

With hydrogen; nickel; In ethanol; for 48h; Ambient temperature;

Reference yield: 44.0%

(5R and 5S)-5,6-anhydro-1,2-O-isopropylidene-5-<(R and S)-(methoxy)phenylphosphinyl>-3-O-methyl-β-D-arabino-hexofuranoses (76707-48-7,77096-94-7,130930-03-9,134356-01-7,134356-02-8) → (5R and 5S)-5,6-dideoxy-1,2-O-isopropylidene-5-<(R and S)-(methoxy)phenylphosphinyl>-3-O-methyl-β-D-arabino-hexofuranoses (66034-26-2,70632-56-3,130930-04-0,134356-03-9,134356-04-0)

Guidance literature:

With hydrogen; nickel;

DOI:10.1246/cl.1990.1359

Reference yield: 25.0%

5,6-anhydro-1,2-O-isopropylidene-5-C-<(methoxy)phenylphosphinyl>-3-O-methyl-α-D-glucofuranose (76707-48-7,77096-94-7,130930-03-9,134356-01-7,134356-02-8) → 5,6-dideoxy-1,2-O-isopropylidene-5-C-<(methoxy)phenylphosphinyl>-3-O-methyl-α-D-glucofuranose (70632-56-3) + [(S)-1-((3aR,5S,6R,6aR)-6-Methoxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-ethyl]-phenyl-phosphinic acid methyl ester (66034-26-2)

Guidance literature:

With hydrogen; nickel; In ethanol; for 48h; Ambient temperature;

upstream raw materials:

(5-RS)-5,6-anhydro-3-O-benzyl-5-C-<(ethoxy)phenylphosphinyl>-1,2-O-isopropylidene-α-D-xylo-hexafuranose

(5R and 5S)-5,6-anhydro-1,2-O-isopropylidene-5-<(R and S)-(methoxy)phenylphosphinyl>-3-O-methyl-β-D-arabino-hexofuranoses

methyl phenylphosphinate

3-O-methyl-1,2-O-isopropylidene-6-O-tosyl-β-D-arabino-hexofuranos-5-ulose

Downstream raw materials:

5,6-Dideoxy-3-O-methyl-5-phenylphosphinyl-D-arabino-hexopyranose

(5R and 5S)-5,6-dideoxy-1,2-O-isopropylidene-3-O-methyl-5-<(R and S)-phenylphosphinyl>-β-D-arabino-hexofuranoses

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