3-Pyridinecarboxylicacid,1,4,5,6-tetrahydro-,methylester(9CI)

Base Information

Chemical Name:3-Pyridinecarboxylicacid,1,4,5,6-tetrahydro-,methylester(9CI)
CAS No.:14997-05-8
Molecular Formula:C7H11 N O2
Molecular Weight:141.17
Hs Code.:2933399090
Mol file:14997-05-8.mol

Synonyms:Nicotinicacid, 1,4,5,6-tetrahydro-, methyl ester (8CI);3-(Methoxycarbonyl)-1,4,5,6-tetrahydropyridine; Methyl1,4,5,6-tetrahydronicotinate

Suppliers and Price of 3-Pyridinecarboxylicacid,1,4,5,6-tetrahydro-,methylester(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Methyl1,4,5,6-Tetrahydropyridine-3-carboxylate
50mg
$ 155.00

SynQuest Laboratories
Methyl 1,4,5,6-tetrahydropyridine-3-carboxylate
1 g
$ 2128.00

Crysdot
Methyl1,4,5,6-tetrahydropyridine-3-carboxylate 95+%
1g
$ 554.00

Alichem
Methyl1,4,5,6-tetrahydropyridine-3-carboxylate
1g
$ 599.20

AK Scientific
Methyl1,4,5,6-tetrahydropyridine-3-carboxylate
1g
$ 1342.00

Total 8 raw suppliers

Chemical Property of 3-Pyridinecarboxylicacid,1,4,5,6-tetrahydro-,methylester(9CI)

Chemical Property:

PSA：38.33000
LogP:0.75550

Purity/Quality:

99%, ^*data from raw suppliers

Methyl1,4,5,6-Tetrahydropyridine-3-carboxylate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Pyridinecarboxylicacid,1,4,5,6-tetrahydro-,methylester(9CI)

There total 6 articles about 3-Pyridinecarboxylicacid,1,4,5,6-tetrahydro-,methylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 93-60-7
methyl 3-pyridinecarboxylate

: 14997-05-8
methyl 1,4,5,6-tetrahydropyridine-3-carboxylate

Guidance literature:: With palladium on activated charcoal; hydrogen; triethylamine; In methanol; at 23 ℃; for 48h;
DOI:10.1021/acs.orglett.0c01242

Reference yield: 61.0%

: ethyl methyl 1-chloropiperidine-3,3-dicarboxylate

: 14997-05-8
methyl 1,4,5,6-tetrahydropyridine-3-carboxylate

Guidance literature:: With sodium; In methanol; for 1h; Heating;
DOI:10.1002/1522-2675(20000809)83:8<1753::AID-HLCA1753>3.0.CO;2-G

Reference yield:

: 304850-59-7
ethyl methyl piperidine-3,3-dicarboxylate

: 14997-05-8
methyl 1,4,5,6-tetrahydropyridine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / N-chlorosuccinimide / CH₂Cl₂ / 12 h / 25 °C

2: 61 percent / Na / methanol / 1 h / Heating

With N-chloro-succinimide; sodium; In methanol; dichloromethane; 1: Chlorination / 2: Elimination;
DOI:10.1002/1522-2675(20000809)83:8<1753::AID-HLCA1753>3.0.CO;2-G