3-methyl-1,2-bis(η5-cyclopentadienyl)-1,2-dicobaltcyclopentane

Base Information

• Chemical Name: 3-methyl-1,2-bis(η5-cyclopentadienyl)-1,2-dicobaltcyclopentane
• CAS No.: 86632-47-5
• Molecular Formula: C₁₆H₁₈Co₂O₂
• Molecular Weight: 360.304

Synonyms:3-methyl-1,2-bis(η5-cyclopentadienyl)-1,2-dicobaltcyclopentane

Chemical Property of 3-methyl-1,2-bis(η5-cyclopentadienyl)-1,2-dicobaltcyclopentane

Chemical Property:

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Technology Process of 3-methyl-1,2-bis(η5-cyclopentadienyl)-1,2-dicobaltcyclopentane

There total 1 articles about 3-methyl-1,2-bis(η5-cyclopentadienyl)-1,2-dicobaltcyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

(+/-)-1,3-diiodobutane (18371-24-9) + bis(triphenylphosphine)nitrogen bis(η5-cyclopentadienyl)bis(μ-carbonyl)dicobaltate → dicarbonylcyclopentadienylcobalt (12078-25-0,12078-23-8) + 3-methyl-1,2-bis(η5-cyclopentadienyl)-1,2-dicobaltcyclopentane (86632-47-5)

Guidance literature:

In tetrahydrofuran; byproducts: NaI; under inert atmosphere, to suspn. of Co complex in THF added 1,3-diiodobutane, stirred for 2 h; hexane added, filtered, solvent removed under vac., residue chromd., solvent removed under vac., recrystd. from toluene/hexane, filtered, washed with cold pentane, dried under vac., elem. anal.;

DOI:10.1021/ja00357a015

upstream raw materials:

(+/-)-1,3-diiodobutane

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