N-[4'-(2-butyl-benzofuran-3-ylmethyl)-4-(3-phenyl-propoxy)-biphenyl-3-yl]-oxalamic acid

Base Information

Chemical Name:N-[4'-(2-butyl-benzofuran-3-ylmethyl)-4-(3-phenyl-propoxy)-biphenyl-3-yl]-oxalamic acid
CAS No.:796071-95-9
Molecular Formula:C₃₆H₃₅NO₅
Molecular Weight:561.678
Hs Code.:

Synonyms:N-[4'-(2-butyl-benzofuran-3-ylmethyl)-4-(3-phenyl-propoxy)-biphenyl-3-yl]-oxalamic acid

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Chemical Property of N-[4'-(2-butyl-benzofuran-3-ylmethyl)-4-(3-phenyl-propoxy)-biphenyl-3-yl]-oxalamic acid

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Technology Process of N-[4'-(2-butyl-benzofuran-3-ylmethyl)-4-(3-phenyl-propoxy)-biphenyl-3-yl]-oxalamic acid

There total 9 articles about N-[4'-(2-butyl-benzofuran-3-ylmethyl)-4-(3-phenyl-propoxy)-biphenyl-3-yl]-oxalamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: N-[4'-(2-butyl-benzofuran-3-ylmethyl)-4-(3-phenyl-propoxy)-biphenyl-3-yl]-oxalamic acid ethyl ester

: 796071-95-9
N-[4'-(2-butyl-benzofuran-3-ylmethyl)-4-(3-phenyl-propoxy)-biphenyl-3-yl]-oxalamic acid

Guidance literature:: With sodium hydroxide; water; In ethanol; at 20 ℃; for 1h;

Reference yield:

: 796072-19-0
3-(4-bromo-benzyl)-2-butyl-benzofuran

: 796071-95-9
N-[4'-(2-butyl-benzofuran-3-ylmethyl)-4-(3-phenyl-propoxy)-biphenyl-3-yl]-oxalamic acid

Guidance literature:: Multi-step reaction with 5 steps

1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 80 °C

2: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; N,N-dimethyl-formamide / 120 °C

3: iron; acetic acid / ethanol / 3 h / 120 °C

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h

5: sodium hydroxide; water / ethanol / 1 h / 20 °C

With sodium hydroxide; water; potassium acetate; iron; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1: Suzuki Coupling / 2: Suzuki Coupling;

Reference yield:

: 289617-51-2
C₁₉H₁₉BrO₂

: 796071-95-9
N-[4'-(2-butyl-benzofuran-3-ylmethyl)-4-(3-phenyl-propoxy)-biphenyl-3-yl]-oxalamic acid

Guidance literature:: Multi-step reaction with 6 steps

1: triethylsilane; trifluoroacetic acid / dichloromethane / 3 h / 0 °C

2: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 80 °C

3: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; N,N-dimethyl-formamide / 120 °C

4: iron; acetic acid / ethanol / 3 h / 120 °C

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h

6: sodium hydroxide; water / ethanol / 1 h / 20 °C

With triethylsilane; sodium hydroxide; water; potassium acetate; iron; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 2: Suzuki Coupling / 3: Suzuki Coupling;