S-Phenyl (2R,3S)-2-ethyl-3-N-(R)-α-methylbenzylamino-5-trimethylsilyl-4-pentynethioate

Base Information

Chemical Name:S-Phenyl (2R,3S)-2-ethyl-3-N-(R)-α-methylbenzylamino-5-trimethylsilyl-4-pentynethioate
CAS No.:121651-90-9
Molecular Formula:C₂₄H₃₁NOSSi
Molecular Weight:409.668
Hs Code.:

Synonyms:S-Phenyl (2R,3S)-2-ethyl-3-N-(R)-α-methylbenzylamino-5-trimethylsilyl-4-pentynethioate

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Chemical Property of S-Phenyl (2R,3S)-2-ethyl-3-N-(R)-α-methylbenzylamino-5-trimethylsilyl-4-pentynethioate

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Technology Process of S-Phenyl (2R,3S)-2-ethyl-3-N-(R)-α-methylbenzylamino-5-trimethylsilyl-4-pentynethioate

There total 3 articles about S-Phenyl (2R,3S)-2-ethyl-3-N-(R)-α-methylbenzylamino-5-trimethylsilyl-4-pentynethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2975-46-4
3-(trimethylsilyl)prop-2-yn-1-al

: 121651-90-9
S-Phenyl (2R,3S)-2-ethyl-3-N-(R)-α-methylbenzylamino-5-trimethylsilyl-4-pentynethioate

Guidance literature:: Multi-step reaction with 2 steps

1: MgSO₄ / benzene

2: 1.) 9-borabicyclo<3.3.1>non-9-yl triflate, diisopropylethylamine / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) 0 to 25 deg C gradually, then 20 h

With magnesium sulfate; N-ethyl-N,N-diisopropylamine; 9-BBN triflate; In benzene;
DOI:10.1016/S0040-4020(01)87042-3

Reference yield:

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 121651-90-9
S-Phenyl (2R,3S)-2-ethyl-3-N-(R)-α-methylbenzylamino-5-trimethylsilyl-4-pentynethioate

Guidance literature:: Multi-step reaction with 2 steps

1: MgSO₄ / benzene

2: 1.) 9-borabicyclo<3.3.1>non-9-yl triflate, diisopropylethylamine / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) 0 to 25 deg C gradually, then 20 h

With magnesium sulfate; N-ethyl-N,N-diisopropylamine; 9-BBN triflate; In benzene;
DOI:10.1016/S0040-4020(01)87042-3

Reference yield:

: 18245-73-3
S-phenyl thio-n-butyrate

: 131852-34-1
(R)-<1-(N-<3-(Trimethylsilyl)-2-propynylidene>amino)ethyl>benzene

: 121651-90-9
S-Phenyl (2R,3S)-2-ethyl-3-N-(R)-α-methylbenzylamino-5-trimethylsilyl-4-pentynethioate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; 9-BBN triflate; Yield given. Multistep reaction; 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) 0 to 25 deg C gradually, then 20 h;
DOI:10.1016/S0040-4020(01)87042-3