Technology Process of 2-Acetyl-5-benzyloxy-1,4-dimethoxynaphthalene
There total 8 articles about 2-Acetyl-5-benzyloxy-1,4-dimethoxynaphthalene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-methyl-2-indolinone; tetrapropylammonium perruthennate;
In
dichloromethane;
for 3h;
DOI:10.1016/S0040-4039(99)02241-8
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 21 percent / Br2; AcOH / CHCl3 / 1.17 h / 0 °C
2.1: 84 percent / Ag2O / CHCl3 / 2 h
3.1: aq. Na2S2O4 / CH2Cl2; diethyl ether / 0.17 h
4.1: 1.12 g / K2CO3 / acetone / 48 h / Heating
5.1: n-BuLi / tetrahydrofuran; hexane / 0.01 h / -78 °C
5.2: 97 percent / tetrahydrofuran; hexane / 1 h / -78 - 20 °C
6.1: 78 percent / TPAP; NMO; 4 Angstroem molecular sieves / CH2Cl2 / 3 h
With
n-butyllithium; sodium dithionite; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; bromine; potassium carbonate; acetic acid; silver(l) oxide;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane; chloroform; acetone;
DOI:10.1039/b102807n
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 84 percent / Ag2O / CHCl3 / 2 h
2.1: aq. Na2S2O4 / CH2Cl2; diethyl ether / 0.17 h
3.1: 1.12 g / K2CO3 / acetone / 48 h / Heating
4.1: n-BuLi / tetrahydrofuran; hexane / 0.01 h / -78 °C
4.2: 97 percent / tetrahydrofuran; hexane / 1 h / -78 - 20 °C
5.1: 78 percent / TPAP; NMO; 4 Angstroem molecular sieves / CH2Cl2 / 3 h
With
n-butyllithium; sodium dithionite; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; potassium carbonate; silver(l) oxide;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane; chloroform; acetone;
DOI:10.1039/b102807n
