2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid

Base Information

Chemical Name:2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid
CAS No.:220759-00-2
Molecular Formula:C₃₄H₄₆N₄O₄
Molecular Weight:574.764
Hs Code.:

2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[<i>cd</i>]indene-6-carboxylic acid

Synonyms:2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid

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Chemical Property of 2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid

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Technology Process of 2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid

There total 3 articles about 2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 220758-99-6
2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester

: 220759-00-2
2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 3h;
DOI:10.1002/(SICI)1521-3773(19981231)37:24<3410::AID-ANIE3410>3.0.CO;2-1

Reference yield:

: 3a,6a-bis-(4-heptyl-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-d]imidazole-2,5-dione

: 220759-00-2
2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / Cs₂CO₃ / acetonitrile / 3 h / Heating

2: 62 percent / CAN / acetonitrile; H₂O / 24 h / Ambient temperature

3: 100 percent / H₂ / Pd/C / ethanol / 3 h

With ammonium cerium(IV) nitrate; hydrogen; caesium carbonate; palladium on activated charcoal; In ethanol; water; acetonitrile;
DOI:10.1002/(SICI)1521-3773(19981231)37:24<3410::AID-ANIE3410>3.0.CO;2-1

Reference yield:

: 220758-98-5
2a,7b-bis-(4-heptyl-phenyl)-2,3-bis-(4-methoxy-benzyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester

: 220759-00-2
2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / CAN / acetonitrile; H₂O / 24 h / Ambient temperature

2: 100 percent / H₂ / Pd/C / ethanol / 3 h

With ammonium cerium(IV) nitrate; hydrogen; palladium on activated charcoal; In ethanol; water; acetonitrile;
DOI:10.1002/(SICI)1521-3773(19981231)37:24<3410::AID-ANIE3410>3.0.CO;2-1