[(2S,3S,4R)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-carboxymethyl-tetrahydro-furan-3-yl]-acetic acid

Base Information

Chemical Name:[(2S,3S,4R)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-carboxymethyl-tetrahydro-furan-3-yl]-acetic acid
CAS No.:109917-94-4
Molecular Formula:C₂₅H₃₂O₆Si
Molecular Weight:456.611
Hs Code.:

Synonyms:[(2S,3S,4R)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-carboxymethyl-tetrahydro-furan-3-yl]-acetic acid

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Chemical Property of [(2S,3S,4R)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-carboxymethyl-tetrahydro-furan-3-yl]-acetic acid

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Technology Process of [(2S,3S,4R)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-carboxymethyl-tetrahydro-furan-3-yl]-acetic acid

There total 8 articles about [(2S,3S,4R)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-carboxymethyl-tetrahydro-furan-3-yl]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 99808-03-4
(1R,6S,7S)-7-diphenyl-t-butylsiloxymethyl-8-oxabicyclo-<4.3.0>non-3-ene

: 109917-94-4
[(2S,3S,4R)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-carboxymethyl-tetrahydro-furan-3-yl]-acetic acid

Guidance literature:: With potassium permanganate; sodium periodate; In water; acetone; Ambient temperature;

Reference yield:

: 99315-76-1
(5S)-5-(tert-butyldiphenylsiloxymethyl)-2(5H)-furanone

: 109917-94-4
[(2S,3S,4R)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-carboxymethyl-tetrahydro-furan-3-yl]-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / AlCl₃ / CH₂Cl₂ / 168 h / 55 °C

2: LiBH₄ / tetrahydrofuran / Ambient temperature

3: 85 percent / tosyl chloride, pyridine / CH₂Cl₂ / -15 °C

4: KMnO₄, NaIO₄ / acetone; H₂O

With pyridine; potassium permanganate; sodium periodate; lithium borohydride; aluminium trichloride; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1039/c39850000737

Reference yield:

: 99315-77-2
(4S,5R)-4-<(S)-2-diphenyl-t-butylsiloxy-1-hydroxyethyl>-5-hydroxymethylcyclohexene

: 109917-94-4
[(2S,3S,4R)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-carboxymethyl-tetrahydro-furan-3-yl]-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / tosyl chloride, pyridine / CH₂Cl₂ / -15 °C

2: KMnO₄, NaIO₄ / acetone; H₂O

With pyridine; potassium permanganate; sodium periodate; p-toluenesulfonyl chloride; In dichloromethane; water; acetone;
DOI:10.1039/c39850000737