3,5-Di-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-6-C-methyl-α-D-gluco-hept-6-eno-1,4-furanose

Base Information

Chemical Name:3,5-Di-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-6-C-methyl-α-D-gluco-hept-6-eno-1,4-furanose
CAS No.:138638-98-9
Molecular Formula:C₂₅H₃₀O₅
Molecular Weight:410.51
Hs Code.:

Synonyms:3,5-Di-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-6-C-methyl-α-D-gluco-hept-6-eno-1,4-furanose

Suppliers and Price of 3,5-Di-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-6-C-methyl-α-D-gluco-hept-6-eno-1,4-furanose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,5-Di-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-6-C-methyl-α-D-gluco-hept-6-eno-1,4-furanose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,5-Di-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-6-C-methyl-α-D-gluco-hept-6-eno-1,4-furanose

There total 4 articles about 3,5-Di-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-6-C-methyl-α-D-gluco-hept-6-eno-1,4-furanose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 138638-96-7
3,5-Di-O-benzyl-1,2-O-isopropylidene-6-bis-C-<(trimethylsilyl)methyl>-α-D-glucofuranose

: 138638-98-9
3,5-Di-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-6-C-methyl-α-D-gluco-hept-6-eno-1,4-furanose

: 138638-97-8
3,5-Di-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-6-C-methylene-7-C-trimethylsilyl-α-D-gluco-hepto-1,4-furanose

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1016/0008-6215(91)80009-C

Reference yield:

: 28713-39-5
3,5-di-O-benzyl-1,2-O-isopropylidene-α-D-glucofuranose

: 138638-98-9
3,5-Di-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-6-C-methyl-α-D-gluco-hept-6-eno-1,4-furanose

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium dichromate / dimethylformamide / 16 h / Ambient temperature

2: diethyl ether

3: 1. Mg, I₂ / 1. ether; 2. ether, a.) 0 deg C, 1 h, b.) 0 deg C to r.t.

4: 11 percent / p-toluenesulfonic acid monohydrate / CH₂Cl₂

With dipyridinium dichromate; iodine; toluene-4-sulfonic acid; magnesium; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(91)80009-C

Reference yield:

: (S)-Benzyloxy-((3aR,5S,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-acetic acid

: 138638-98-9
3,5-Di-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-6-C-methyl-α-D-gluco-hept-6-eno-1,4-furanose

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: 1. Mg, I₂ / 1. ether; 2. ether, a.) 0 deg C, 1 h, b.) 0 deg C to r.t.

3: 11 percent / p-toluenesulfonic acid monohydrate / CH₂Cl₂

With iodine; toluene-4-sulfonic acid; magnesium; In diethyl ether; dichloromethane;
DOI:10.1016/0008-6215(91)80009-C