(+/-)-3,3,6,6-tetramethyl-9-phenyl-1-oxa-4,7-diazacyclononan-2,5,8-trion

Base Information

Chemical Name:(+/-)-3,3,6,6-tetramethyl-9-phenyl-1-oxa-4,7-diazacyclononan-2,5,8-trion
CAS No.:87872-96-6
Molecular Formula:C₁₆H₂₀N₂O₄
Molecular Weight:304.346
Hs Code.:

Synonyms:(+/-)-3,3,6,6-tetramethyl-9-phenyl-1-oxa-4,7-diazacyclononan-2,5,8-trion

Suppliers and Price of (+/-)-3,3,6,6-tetramethyl-9-phenyl-1-oxa-4,7-diazacyclononan-2,5,8-trion

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-3,3,6,6-tetramethyl-9-phenyl-1-oxa-4,7-diazacyclononan-2,5,8-trion

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-3,3,6,6-tetramethyl-9-phenyl-1-oxa-4,7-diazacyclononan-2,5,8-trion

There total 3 articles about (+/-)-3,3,6,6-tetramethyl-9-phenyl-1-oxa-4,7-diazacyclononan-2,5,8-trion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 87866-93-1
(+/-)-2-<2-(2-hydroxy-2-phenylacetamido)-2-methylpropionamido>-N,N,2-trimethylpropionamid

: 87872-96-6
(+/-)-3,3,6,6-tetramethyl-9-phenyl-1-oxa-4,7-diazacyclononan-2,5,8-trion

Guidance literature:: With hydrogenchloride; In toluene; at 90 ℃; for 0.0833333h;
DOI:10.1016/S0040-4039(00)81806-7

Reference yield:

: 111492-26-3
(+/-)-2-(2-hydroxy-2-phenylacetamido)-2-methylpropionsaure

: 87872-96-6
(+/-)-3,3,6,6-tetramethyl-9-phenyl-1-oxa-4,7-diazacyclononan-2,5,8-trion

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / acetonitrile / 2 h / Ambient temperature

2: 85 percent / HCl / toluene / 0.08 h / 100 °C

With hydrogenchloride; In toluene; acetonitrile;
DOI:10.1002/hlca.19870700209

Reference yield:

: 111492-13-8
(+/-)-2-(2-hydroxy-2-phenylacetamido)-N,N,2-trimethylpropionamid

: 87872-96-6
(+/-)-3,3,6,6-tetramethyl-9-phenyl-1-oxa-4,7-diazacyclononan-2,5,8-trion

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / HCl / acetonitrile; H₂O / 0.17 h / 60 - 70 °C

2: 93 percent / acetonitrile / 2 h / Ambient temperature

3: 85 percent / HCl / toluene / 0.08 h / 100 °C

With hydrogenchloride; In water; toluene; acetonitrile;
DOI:10.1002/hlca.19870700209