3-Benzyloxy-4-methyl-2-nitro-N-[(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-methyl]-benzamide

Base Information

Chemical Name:3-Benzyloxy-4-methyl-2-nitro-N-[(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-methyl]-benzamide
CAS No.:211674-36-1
Molecular Formula:C₃₁H₃₅N₃O₁₀
Molecular Weight:609.633
Hs Code.:

Synonyms:3-Benzyloxy-4-methyl-2-nitro-N-[(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-methyl]-benzamide

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Chemical Property of 3-Benzyloxy-4-methyl-2-nitro-N-[(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-methyl]-benzamide

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Technology Process of 3-Benzyloxy-4-methyl-2-nitro-N-[(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-methyl]-benzamide

There total 5 articles about 3-Benzyloxy-4-methyl-2-nitro-N-[(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-methyl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 60835-71-4
4'-aminobenzo-15-crown-5-ether

: (3-Benzyloxy-4-methyl-2-nitro-benzoylamino)-acetyl azide

: 211674-36-1
3-Benzyloxy-4-methyl-2-nitro-N-[(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-methyl]-benzamide

Guidance literature:: In diethyl ether; chloroform; at 18 ℃; for 20h;

Reference yield:

: 60835-69-0
4'-nitrobenzo-15-crown-5

: 211674-36-1
3-Benzyloxy-4-methyl-2-nitro-N-[(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-methyl]-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / dioxane / 18 °C

2: 70 percent / diethyl ether; CHCl₃ / 20 h / 18 °C

With hydrogen; palladium on activated charcoal; In 1,4-dioxane; diethyl ether; chloroform;

Reference yield:

: 7536-35-8
2-nitro-3-benzyloxy-4-methylbenzoyl chloride

: 211674-36-1
3-Benzyloxy-4-methyl-2-nitro-N-[(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-ylcarbamoyl)-methyl]-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / Et₃N / CHCl₃ / 22 h / 18 °C

2: 97 percent / N₂H₄*H₂O / ethanol / 20 h / 18 °C

3: HCl, NaNO₂ / aq. acetic acid

4: 70 percent / diethyl ether; CHCl₃ / 20 h / 18 °C

With hydrogenchloride; hydrazine hydrate; triethylamine; sodium nitrite; In diethyl ether; ethanol; chloroform; acetic acid;