[2,2'-bis(dipentafluorophenylphosphino)diphenyl oxide]palladium dichloride

Base Information

Chemical Name:[2,2'-bis(dipentafluorophenylphosphino)diphenyl oxide]palladium dichloride
CAS No.:878293-70-0
Molecular Formula:C₃₆H₈Cl₂F₂₀OP₂Pd
Molecular Weight:1075.7
Hs Code.:

Synonyms:[2,2'-bis(dipentafluorophenylphosphino)diphenyl oxide]palladium dichloride

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Chemical Property of [2,2'-bis(dipentafluorophenylphosphino)diphenyl oxide]palladium dichloride

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Technology Process of [2,2'-bis(dipentafluorophenylphosphino)diphenyl oxide]palladium dichloride

There total 1 articles about [2,2'-bis(dipentafluorophenylphosphino)diphenyl oxide]palladium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 434336-18-2
2,2'-bis[bis(pentafluorophenyl)phosphino]diphenyl ether

: 878293-70-0
[2,2'-bis(dipentafluorophenylphosphino)diphenyl oxide]palladium dichloride

Guidance literature:: In tetrahydrofuran; byproducts: benzonitrile; (Ar); placing of (C6H4P(C6F5)2)2O in flask; addn. of soln. of PdCl2(PhCN)2 in THF with stirring, pptn., stirring for 4 h at 60°C; standing overnight, removal of solvent in vac., dissolving in CH2Cl2 or benzene, treatment with hexane, pptn., washing with ether, drying in vac., elem. anal.;
DOI:10.1007/s11176-005-0199-9