(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-indole

Base Information

Chemical Name:(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-indole
CAS No.:85923-67-7
Molecular Formula:C₂₄H₂₈N₂O₃S
Molecular Weight:424.564
Hs Code.:

(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-<N-(4-ethyl-4-pentenyl)formimidoyl>indole

Synonyms:(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-indole

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Chemical Property of (E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-indole

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Technology Process of (E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-indole

There total 5 articles about (E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5416-80-8
2-methyl-1H-indole-3-carbaldehyde

: 85923-67-7
(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-indole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride, 2.) imidazole / 1.) glyme, 20 deg C, 1.5 h, reflux, 15 min, 2.) 20 deg C, 15 h

2: CH₂Cl₂ / 15 h / 4 Angstroem molecular sieves

With 1H-imidazole; sodium hydride; In dichloromethane;
DOI:10.1021/ja00352a037

Reference yield:

: 13722-73-1
4-ethylpent-4-enoic acid

: 85923-67-7
(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-indole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) triethylamine, 2.) ethyl chloroformate, 3.) ammonia / 1.) dichloromethane, 0 deg C, 10 min, 2.) 0 deg C, 1 h, 0 deg C -> 20 deg c, 0.5 h, 3.) 20 deg C, 15 h

2: 49 percent / lithium aluminum hydride / diethyl ether / 15 h / 20 °C

3: CH₂Cl₂ / 15 h / 4 Angstroem molecular sieves

With lithium aluminium tetrahydride; ammonia; chloroformic acid ethyl ester; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/ja00352a037

Reference yield:

: 4-ethyl-4-pentenamide

: 85923-67-7
(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-indole

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / lithium aluminum hydride / diethyl ether / 15 h / 20 °C

2: CH₂Cl₂ / 15 h / 4 Angstroem molecular sieves

With lithium aluminium tetrahydride; In diethyl ether; dichloromethane;
DOI:10.1021/ja00352a037