Technology Process of C24H40O5Si
There total 5 articles about C24H40O5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
acetic acid tert-butyl ester;
With
lithium diisopropyl amide;
In
tetrahydrofuran;
at -78 ℃;
for 1h;
C22H38O3SSi;
In
tetrahydrofuran;
at -78 - 0 ℃;
for 2h;
DOI:10.1055/s-0030-1260784
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diisobutylaluminium hydride / diethyl ether / 1.5 h / -78 °C
2.1: tin(IV) chloride / dichloromethane / 1 h / -78 °C
3.1: 1H-imidazole / N,N-dimethyl-formamide / 2.5 h / 20 °C
4.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C
4.2: 2 h / -78 - 0 °C
With
1H-imidazole; tin(IV) chloride; diisobutylaluminium hydride; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-0030-1260784
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 5 h / 0 - 20 °C
2.1: diisobutylaluminium hydride / diethyl ether / 1.5 h / -78 °C
3.1: tin(IV) chloride / dichloromethane / 1 h / -78 °C
4.1: 1H-imidazole / N,N-dimethyl-formamide / 2.5 h / 20 °C
5.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C
5.2: 2 h / -78 - 0 °C
With
1H-imidazole; trimethylsilyl trifluoromethanesulfonate; tin(IV) chloride; diisobutylaluminium hydride; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-0030-1260784
