2-((2',6'-dimethoxybiphenyl-4-yl)carbonyl)phenyl trifluoromethanesulfonate

Base Information

Chemical Name:2-((2',6'-dimethoxybiphenyl-4-yl)carbonyl)phenyl trifluoromethanesulfonate
CAS No.:1353010-53-3
Molecular Formula:C₂₂H₁₇F₃O₆S
Molecular Weight:466.435
Hs Code.:

Synonyms:2-((2',6'-dimethoxybiphenyl-4-yl)carbonyl)phenyl trifluoromethanesulfonate

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Chemical Property of 2-((2',6'-dimethoxybiphenyl-4-yl)carbonyl)phenyl trifluoromethanesulfonate

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Technology Process of 2-((2',6'-dimethoxybiphenyl-4-yl)carbonyl)phenyl trifluoromethanesulfonate

There total 2 articles about 2-((2',6'-dimethoxybiphenyl-4-yl)carbonyl)phenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1353010-46-4
2-[4-(trifluoromethanesulfonyloxy)benzoyl]phenyl trifluoromethanesulfonate

: 23112-96-1
(2,6-dimethoxyphenyl)boronic acid

: 1353010-53-3
2-((2',6'-dimethoxybiphenyl-4-yl)carbonyl)phenyl trifluoromethanesulfonate

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 110 ℃; for 4h; regioselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201100762

Reference yield:

: 606-12-2
4-[(2-hydroxyphenyl)carbonyl]phenol

: 1353010-53-3
2-((2',6'-dimethoxybiphenyl-4-yl)carbonyl)phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 0.17 h / -78 °C / Inert atmosphere

1.2: 4 h / -78 - 0 °C / Inert atmosphere

2.1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 4 h / 110 °C / Inert atmosphere

With pyridine; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; 2.1: Suzuki coupling;
DOI:10.1002/ejoc.201100762

Reference yield: 68.0%

: 1353010-53-3
2-((2',6'-dimethoxybiphenyl-4-yl)carbonyl)phenyl trifluoromethanesulfonate

: 2156-04-9,593231-72-2
4-Vinylphenylboronic acid

: 1353010-61-3
(2',6'-dimethoxybiphenyl-4-yl)(4'-vinylbiphenyl-2-yl)methanone

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 110 ℃; for 4h; Inert atmosphere;
DOI:10.1002/ejoc.201100762