2-Decaprenyl-3-methyl-6-methoxy-1,4-benzoquinone

Base Information

• Chemical Name: 2-Decaprenyl-3-methyl-6-methoxy-1,4-benzoquinone
• CAS No.: 14599-49-6
• Molecular Formula: C58H88 O4
• Molecular Weight: 849.32
• Mol file: 14599-49-6.mol

Synonyms:Benzoquinone,2-(3,7,11,15,19,23,27,31,35,39-decamethyl-2,6,10,14,18,22,26,30,34,38-tetracontadecaenyl)-5-hydroxy-6-methoxy-3-methyl-(8CI); 2-Decaprenyl-5-hydroxy-6-methoxy-3-methyl-1,4-benzoquinone

Chemical Property of 2-Decaprenyl-3-methyl-6-methoxy-1,4-benzoquinone

Chemical Property:

• Vapor Pressure: 3.95E-34mmHg at 25°C
• Refractive Index: 1.532
• Boiling Point: 856.1°C at 760 mmHg
• Flash Point: 223.9°C
• PSA: 63.60000
• Density: 0.98g/cm³
• LogP: 17.76550

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Decaprenyl-3-methyl-6-methoxy-1,4-benzoquinone

There total 4 articles about 2-Decaprenyl-3-methyl-6-methoxy-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-demethoxyubiquinone-10 (7200-27-3,47904-52-9) → 2-Hydroxy-3-methoxy-6-methyl-5-decaprenyl-1,4-benzochinon (14599-49-6)

Guidance literature:

Multi-step reaction with 2 steps

1: NH₃ / diethyl ether; methanol

2: CuCl₂*2H₂O / acetic acid / Heating

With ammonia; CuCl₂*2H₂O; In methanol; diethyl ether; acetic acid;

DOI:10.1021/ja01022a050

Reference yield:

3,7,11,15,19,23,27,31,35,39-decamethyl-1,6,10,14,18,22,26,30,34,38-tetracontadecaene-3-ol (59640-02-7) → 2-Hydroxy-3-methoxy-6-methyl-5-decaprenyl-1,4-benzochinon (14599-49-6)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) NaHSO₃, Et₂O, (ii) /BRN= 3115762/, BF₃-Et₂O, dioxane

2: NH₃ / diethyl ether; methanol

3: CuCl₂*2H₂O / acetic acid / Heating

With ammonia; CuCl₂*2H₂O; In methanol; diethyl ether; acetic acid;

DOI:10.1021/ja01022a050

Reference yield:

(all-E)-3,7,11,15,19,23,27,31,35,39-decamethyl-tetraconta-6,10,14,18,22,26,30,34,38-nonaen-1-yn-3-ol → 2-Hydroxy-3-methoxy-6-methyl-5-decaprenyl-1,4-benzochinon (14599-49-6)

Guidance literature:

Multi-step reaction with 4 steps

1: (reduction)

2: (i) NaHSO₃, Et₂O, (ii) /BRN= 3115762/, BF₃-Et₂O, dioxane

3: NH₃ / diethyl ether; methanol

4: CuCl₂*2H₂O / acetic acid / Heating

With ammonia; CuCl₂*2H₂O; In methanol; diethyl ether; acetic acid;

DOI:10.1021/ja01022a050

upstream raw materials:

5-demethoxyubiquinone-10

3,7,11,15,19,23,27,31,35,39-decamethyl-1,6,10,14,18,22,26,30,34,38-tetracontadecaene-3-ol