[Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)₃]

Base Information

• Chemical Name: [Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)₃]
• CAS No.: 1601494-25-0
• Molecular Formula: C₃₄H₂₉MoN₃O₃P₂
• Molecular Weight: 685.51
• Mol file: 1601494-25-0.mol

Synonyms:[Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)₃]

Chemical Property of [Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)₃]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)₃]

There total 1 articles about [Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)₃] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N,N′-bis(diphenylphosphino)-N,N′-dimethyl-2,6-diaminopyridine (1601494-24-9) + molybdenum hexacarbonyl (13939-06-5,199620-15-0) → [Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)3] (1601494-25-0)

Guidance literature:

molybdenum hexacarbonyl; In acetonitrile; for 3h; Reflux; Inert atmosphere;

N,N′-bis(diphenylphosphino)-N,N′-dimethyl-2,6-diaminopyridine; In toluene; acetonitrile; at 20 ℃; for 96h; Inert atmosphere; Reflux;

DOI:10.1016/j.jorganchem.2013.12.018

Reference yield: 93.0%

[Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)3] (1601494-25-0) + 1-fluoro-2,4,6-trimethylpyridin-1-ium tetrafluoroborate → [Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)2F2] (1601494-29-4)

Guidance literature:

In dichloromethane; for 72h; Inert atmosphere;

DOI:10.1016/j.jorganchem.2013.12.018

Reference yield:

[Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)3] (1601494-25-0) + iodine (7553-56-2,12190-71-5,8031-47-8) → [Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)2I2] (1601494-26-1)

Guidance literature:

In acetonitrile; at -78 - 20 ℃; for 18h; Inert atmosphere;

DOI:10.1016/j.jorganchem.2013.12.018

upstream raw materials:

N,N′-bis(diphenylphosphino)-N,N′-dimethyl-2,6-diaminopyridine

molybdenum hexacarbonyl

Downstream raw materials:

[Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)₂I₂]

[Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)₂Br₂]

[Mo(N,N′-bis(diphenylphosphino)-N,N′-methyl-2,6-diaminopyridine)(CO)₂F₂]