N-(β-D-glucopyranosyl)-1-(3,5-dimethylphenyl)-1,2,3-triazole-4-carboxamide

Base Information

Chemical Name:N-(β-D-glucopyranosyl)-1-(3,5-dimethylphenyl)-1,2,3-triazole-4-carboxamide
CAS No.:1366651-42-4
Molecular Formula:C₁₇H₂₂N₄O₆
Molecular Weight:378.385
Hs Code.:

Synonyms:N-(β-D-glucopyranosyl)-1-(3,5-dimethylphenyl)-1,2,3-triazole-4-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(β-D-glucopyranosyl)-1-(3,5-dimethylphenyl)-1,2,3-triazole-4-carboxamide

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Technology Process of N-(β-D-glucopyranosyl)-1-(3,5-dimethylphenyl)-1,2,3-triazole-4-carboxamide

There total 5 articles about N-(β-D-glucopyranosyl)-1-(3,5-dimethylphenyl)-1,2,3-triazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1366651-33-3
N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1-(3,5-dimethylphenyl)-1,2,3-triazole-4-carboxamide

: 1366651-42-4
N-(β-D-glucopyranosyl)-1-(3,5-dimethylphenyl)-1,2,3-triazole-4-carboxamide

Guidance literature:: With methanol; sodium methylate; at 20 ℃; for 1h;
DOI:10.1016/j.carres.2012.01.020

Reference yield:

: 41355-50-4,51642-81-0,58484-22-3,70128-27-7,70145-20-9,94482-21-0,98300-76-6
2,3,4,6-tetra-O-acetyl-D-glucosyl-1-amine

: 1366651-42-4
N-(β-D-glucopyranosyl)-1-(3,5-dimethylphenyl)-1,2,3-triazole-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexyl-carbodiimide / dichloromethane / 20 °C

2: copper(ll) sulfate pentahydrate; ascorbic acid / methanol; dichloromethane; water / 50 °C

3: methanol; sodium methylate / 1 h / 20 °C

With methanol; copper(ll) sulfate pentahydrate; sodium methylate; dicyclohexyl-carbodiimide; ascorbic acid; In methanol; dichloromethane; water; 3: Zemplen deacylation;
DOI:10.1016/j.carres.2012.01.020

Reference yield:

: 172975-69-8
3,5-dimethylphenyl boronic acid

: 1366651-42-4
N-(β-D-glucopyranosyl)-1-(3,5-dimethylphenyl)-1,2,3-triazole-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: copper(ll) sulfate pentahydrate; sodium azide / methanol / 20 °C

2: copper(ll) sulfate pentahydrate; ascorbic acid / methanol; dichloromethane; water / 50 °C

3: methanol; sodium methylate / 1 h / 20 °C

With methanol; sodium azide; copper(ll) sulfate pentahydrate; sodium methylate; ascorbic acid; In methanol; dichloromethane; water; 3: Zemplen deacylation;
DOI:10.1016/j.carres.2012.01.020