[4-((2R,6R)-2,6,10-Trimethyl-undecyloxycarbonylamino)-phenyl]-carbamic acid (2R,6R)-2,6,10-trimethyl-undecyl ester

Base Information

Chemical Name:[4-((2R,6R)-2,6,10-Trimethyl-undecyloxycarbonylamino)-phenyl]-carbamic acid (2R,6R)-2,6,10-trimethyl-undecyl ester
CAS No.:376635-21-1
Molecular Formula:C₃₆H₆₄N₂O₄
Molecular Weight:588.915
Hs Code.:

Synonyms:[4-((2R,6R)-2,6,10-Trimethyl-undecyloxycarbonylamino)-phenyl]-carbamic acid (2R,6R)-2,6,10-trimethyl-undecyl ester

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Chemical Property of [4-((2R,6R)-2,6,10-Trimethyl-undecyloxycarbonylamino)-phenyl]-carbamic acid (2R,6R)-2,6,10-trimethyl-undecyl ester

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Technology Process of [4-((2R,6R)-2,6,10-Trimethyl-undecyloxycarbonylamino)-phenyl]-carbamic acid (2R,6R)-2,6,10-trimethyl-undecyl ester

There total 2 articles about [4-((2R,6R)-2,6,10-Trimethyl-undecyloxycarbonylamino)-phenyl]-carbamic acid (2R,6R)-2,6,10-trimethyl-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 54154-25-5
(2R,6R)-2,6,10-trimethyl-undecan-1-ol

: 104-49-4
1,4-diisocyanatobenzene

: 376635-21-1
[4-((2R,6R)-2,6,10-Trimethyl-undecyloxycarbonylamino)-phenyl]-carbamic acid (2R,6R)-2,6,10-trimethyl-undecyl ester

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In benzene; at 60 ℃; for 3h;
DOI:10.1021/ol010142d

Reference yield:

: 104256-36-2
6,10-dimethyl-undec-1-ene

: 376635-21-1
[4-((2R,6R)-2,6,10-Trimethyl-undecyloxycarbonylamino)-phenyl]-carbamic acid (2R,6R)-2,6,10-trimethyl-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: (-)-(NMI)2ZrCl₂ / CH₂Cl₂ / 23 °C

1.2: O₂ / CH₂Cl₂

2.1: 34 percent / DABCO / benzene / 3 h / 60 °C

With 1,4-diaza-bicyclo[2.2.2]octane; (-)-(NMI)2ZrCl₂; In dichloromethane; benzene;
DOI:10.1021/ol010142d