2,3-O-(1-methylethylidene)-1,6-bis-O-[(4-methylphenyl)sulfonyl]hex-2-ulofuranose

Base Information

• Chemical Name: 2,3-O-(1-methylethylidene)-1,6-bis-O-[(4-methylphenyl)sulfonyl]hex-2-ulofuranose
• CAS No.: 32087-60-8
• Molecular Formula: C23H28 O10 S2
• Molecular Weight: 528.5924

Synonyms:Fructofuranose,2,3-O-isopropylidene-, 1,6-di-p-toluenesulfonate, b-D- (7CI,8CI); Furo[2,3-d]-1,3-dioxole, b-D-fructofuranose deriv.;2,3-O-Isopropylidene-1,6-di-O-p-toluenesulfonyl-b-D-fructofuranose; Fructofuranose,2,3-O-isopropylidene-, 1,6-di-b-toluenesulfonate, b-D-; NSC 170117

Chemical Property of 2,3-O-(1-methylethylidene)-1,6-bis-O-[(4-methylphenyl)sulfonyl]hex-2-ulofuranose

Chemical Property:

• Vapor Pressure: 5.37E-20mmHg at 25°C
• Boiling Point: 690.1°Cat760mmHg
• Flash Point: 371.2°C
• Density: 1.369g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-O-(1-methylethylidene)-1,6-bis-O-[(4-methylphenyl)sulfonyl]hex-2-ulofuranose

There total 3 articles about 2,3-O-(1-methylethylidene)-1,6-bis-O-[(4-methylphenyl)sulfonyl]hex-2-ulofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-Fructose (57-48-7,18875-34-8) + p-toluenesulfonyl chloride (98-59-9) → 2,3-O-isopropylidene-1,6-bis-O-(p-tolylsulphonyl)-β-D-fructofuranose (32087-60-8)

Guidance literature:

With pyridine; chloroform; Behandeln des Reaktionsprodukts mit Aceton, Kupfer(II)-sulfat und wenig Schwefelsaeure;

DOI:10.1002/hlca.193802101132

Reference yield:

p-toluenesulfonyl chloride (98-59-9) + 2,3-O-isopropylidene-β-D-fructofuranose (192573-40-3) → 2,3-O-isopropylidene-1,6-bis-O-(p-tolylsulphonyl)-β-D-fructofuranose (32087-60-8)

Guidance literature:

With pyridine; chloroform;

DOI:10.1002/hlca.193802101132

Reference yield:

→ 2,3-O-isopropylidene-1,6-bis-O-(p-tolylsulphonyl)-β-D-fructofuranose (32087-60-8)

Guidance literature:

aus 1,6-Di-O-p-Toluolsulfonyl-D-fructofuranose;

upstream raw materials:

D-Fructose

p-toluenesulfonyl chloride

2,3-O-isopropylidene-β-D-fructofuranose

Downstream raw materials:

2,3-O-Isopropylidene-4-O-methyl-1,6-di-O-tosyl-β-D-fructofuranose

methyl 1,6-di-O-p-toluenesulfonyl-α-D-fructofuranoside

6-deoxy-6-iodo-2,3-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

methyl 1,6-di-O-p-toluenesulfonyl-β-D-fructofuranoside

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