(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-p-tolylacrylate

Base Information

Chemical Name:(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-p-tolylacrylate
CAS No.:1403877-23-5
Molecular Formula:C₂₄H₂₆O₆
Molecular Weight:410.467
Hs Code.:

Synonyms:(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-p-tolylacrylate

Suppliers and Price of (E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-p-tolylacrylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-p-tolylacrylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-p-tolylacrylate

There total 5 articles about (E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-p-tolylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1866-39-3,940-61-4
trans-p-methylcinnamic acid

: 1322088-10-7
allyl 3-(3,4-dimethoxyphenyl)-2-hydroxypropanoate

: 1403877-23-5
(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-p-tolylacrylate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2012.09.047

Reference yield:

: 143815-52-5
(Z)-3-(3,4-dimethoxyphenyl)-2-hydroxyacrylic acid

: 1403877-23-5
(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-p-tolylacrylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; sodium tetrahydroborate / methanol / 0 - 20 °C / pH 10

2: toluene-4-sulfonic acid / toluene / 10 h / 100 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / 20 °C

With dmap; sodium tetrahydroborate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane; toluene;
DOI:10.1016/j.ejmech.2012.09.047

Reference yield:

: 32255-79-1
2-hydroxy-3-(3,4-dimethoxyphenyl)propanoic acid

: 1403877-23-5
(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-p-tolylacrylate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 10 h / 100 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / 20 °C

With dmap; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; toluene;
DOI:10.1016/j.ejmech.2012.09.047