C₂₄H₂₃ClN₂O₄S

Base Information

Chemical Name:C₂₄H₂₃ClN₂O₄S
CAS No.:1473358-21-2
Molecular Formula:C₂₄H₂₃ClN₂O₄S
Molecular Weight:470.977
Hs Code.:

C<sub>24</sub>H<sub>23</sub>ClN<sub>2</sub>O<sub>4</sub>S

Synonyms:C₂₄H₂₃ClN₂O₄S

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Chemical Property of C₂₄H₂₃ClN₂O₄S

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Technology Process of C₂₄H₂₃ClN₂O₄S

There total 4 articles about C₂₄H₂₃ClN₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1473358-19-8
C₂₅H₃₂BClN₂O₅

: 1473358-21-2
C₂₄H₂₃ClN₂O₄S

Guidance literature:: With potassium fluoride; palladium; In methanol; for 5h; Reflux;
DOI:10.5012/bkcs.2013.34.8.2249

Reference yield:

: 327046-79-7
tert-butyl (4-bromo-2-nitrophenyl)carbamate

: 1473358-21-2
C₂₄H₂₃ClN₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 80 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C / 2585.81 Torr

3: triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

4: palladium; potassium fluoride / methanol / 5 h / Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; palladium 10% on activated carbon; hydrogen; potassium acetate; palladium; triethylamine; In 1,4-dioxane; methanol; dichloromethane; ethyl acetate; 4: |Suzuki Coupling;
DOI:10.5012/bkcs.2013.34.8.2249

Reference yield:

: 855738-60-2
tert-butyl 2-nitro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenylcarbamate

: 1473358-21-2
C₂₄H₂₃ClN₂O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C / 2585.81 Torr

2: triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3: palladium; potassium fluoride / methanol / 5 h / Reflux

With potassium fluoride; palladium 10% on activated carbon; hydrogen; palladium; triethylamine; In methanol; dichloromethane; ethyl acetate; 3: |Suzuki Coupling;
DOI:10.5012/bkcs.2013.34.8.2249