Technology Process of C32H24N2O4S
There total 3 articles about C32H24N2O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium acetate; palladium diacetate;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 4h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 2 h / 40 °C / Inert atmosphere
2: palladium diacetate; potassium acetate / N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; potassium acetate; palladium diacetate;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: bromine; hydrogen bromide / 16 h / 120 °C
2: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 2 h / 40 °C / Inert atmosphere
3: palladium diacetate; potassium acetate / N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; hydrogen bromide; bromine; potassium acetate; palladium diacetate;
In
N,N-dimethyl-formamide;