Technology Process of C18H25NO5
There total 1 articles about C18H25NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 0 - 60 ℃;
DOI:10.1039/c1cc14573h
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 2h;
DOI:10.1039/c1cc14573h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
2: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C
3: 2,4,6-trimethyl-pyridine; manganese; bis(cyclopentadienyl)titanium dichloride; chloro-trimethyl-silane; triphenylphosphine; palladium dichloride / tetrahydrofuran / 21 h / 20 °C / Inert atmosphere
With
2,4,6-trimethyl-pyridine; bis(cyclopentadienyl)titanium dichloride; manganese; chloro-trimethyl-silane; sodium hydride; triphenylphosphine; trifluoroacetic acid; palladium dichloride;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
3: Michael type addition;
DOI:10.1039/c1cc14573h