N-(2-cyclohexyl-1-methyl-6-morpholino-1H-benzo[d]imidazol-5-yl)-5-nitrofuran-2-carboxamide

Base Information

Chemical Name:N-(2-cyclohexyl-1-methyl-6-morpholino-1H-benzo[d]imidazol-5-yl)-5-nitrofuran-2-carboxamide
CAS No.:1465825-87-9
Molecular Formula:C₂₃H₂₇N₅O₅
Molecular Weight:453.498
Hs Code.:

Synonyms:N-(2-cyclohexyl-1-methyl-6-morpholino-1H-benzo[d]imidazol-5-yl)-5-nitrofuran-2-carboxamide

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Chemical Property of N-(2-cyclohexyl-1-methyl-6-morpholino-1H-benzo[d]imidazol-5-yl)-5-nitrofuran-2-carboxamide

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Technology Process of N-(2-cyclohexyl-1-methyl-6-morpholino-1H-benzo[d]imidazol-5-yl)-5-nitrofuran-2-carboxamide

There total 5 articles about N-(2-cyclohexyl-1-methyl-6-morpholino-1H-benzo[d]imidazol-5-yl)-5-nitrofuran-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25084-14-4
5-nitrofuran-2-carboxylic chloride

: 1580534-86-6
C₁₈H₂₆N₄O

: 1465825-87-9
N-(2-cyclohexyl-1-methyl-6-morpholino-1H-benzo[d]imidazol-5-yl)-5-nitrofuran-2-carboxamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.ejmech.2014.01.039

Reference yield:

: 925702-74-5
C₁₀H₁₀FN₃O₅

: 1465825-87-9
N-(2-cyclohexyl-1-methyl-6-morpholino-1H-benzo[d]imidazol-5-yl)-5-nitrofuran-2-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

2: ammonium formate; palladium 10% on activated carbon / tetrahydrofuran; ethanol

3: acetic acid / tetrahydrofuran; ethanol; 1,4-dioxane / 20 °C

4: triethylamine / dichloromethane / 20 °C

With palladium 10% on activated carbon; ammonium formate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane;
DOI:10.1016/j.ejmech.2014.01.039

Reference yield:

: 1580534-65-1
C₁₁H₁₄N₄O₅

: 1465825-87-9
N-(2-cyclohexyl-1-methyl-6-morpholino-1H-benzo[d]imidazol-5-yl)-5-nitrofuran-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium formate; palladium 10% on activated carbon / tetrahydrofuran; ethanol

2: acetic acid / tetrahydrofuran; ethanol; 1,4-dioxane / 20 °C

3: triethylamine / dichloromethane / 20 °C

With palladium 10% on activated carbon; ammonium formate; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane;
DOI:10.1016/j.ejmech.2014.01.039