2-iodoethyl phenoxyacetate

Base Information

• Chemical Name: 2-iodoethyl phenoxyacetate
• CAS No.: 39257-73-3
• Molecular Formula: C₁₀H₁₁IO₃
• Molecular Weight: 306.1
• Mol file: 39257-73-3.mol

Synonyms:2-iodoethyl phenoxyacetate

Chemical Property of 2-iodoethyl phenoxyacetate

Chemical Property:

Purity/Quality:

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Technology Process of 2-iodoethyl phenoxyacetate

There total 1 articles about 2-iodoethyl phenoxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2-iodoethyl phenoxyacetate (39257-73-3)

Guidance literature:

entspr. Carbonylchlorid, HOCH2CH2I in Ggw. v. NEt3/C6H6;

Reference yield: 87.5%

2-iodoethyl phenoxyacetate (39257-73-3) + 5'-O-(4,4'-dimethoxytrityl)-3'-O-(t-butyldimethylsilyl)-2'-deoxythymidine (80971-33-1) → phenoxy-acetic acid 2-{3-[5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tert-butyl-dimethyl-silanyloxy)-tetrahydro-furan-2-yl]-5-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl}-ethyl ester (749254-11-3)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; for 24h;

DOI:10.1021/ja0498540

Downstream raw materials:

phenoxy-acetic acid 2-{3-[5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tert-butyl-dimethyl-silanyloxy)-tetrahydro-furan-2-yl]-5-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl}-ethyl ester