(4R,5S)-1,5-Dimethyl-3-((S)-2-methyl-pent-4-enoyl)-4-phenyl-imidazolidin-2-one

Base Information

Chemical Name:(4R,5S)-1,5-Dimethyl-3-((S)-2-methyl-pent-4-enoyl)-4-phenyl-imidazolidin-2-one
CAS No.:1027396-71-9
Molecular Formula:C₁₇H₂₂N₂O₂
Molecular Weight:286.374
Hs Code.:

Synonyms:(4R,5S)-1,5-Dimethyl-3-((S)-2-methyl-pent-4-enoyl)-4-phenyl-imidazolidin-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5S)-1,5-Dimethyl-3-((S)-2-methyl-pent-4-enoyl)-4-phenyl-imidazolidin-2-one

Chemical Property:

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Technology Process of (4R,5S)-1,5-Dimethyl-3-((S)-2-methyl-pent-4-enoyl)-4-phenyl-imidazolidin-2-one

There total 1 articles about (4R,5S)-1,5-Dimethyl-3-((S)-2-methyl-pent-4-enoyl)-4-phenyl-imidazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112712-55-7
deux références XF130 et XF154

: 106-95-6
allyl bromide

: 1027396-71-9
(4R,5S)-1,5-Dimethyl-3-((S)-2-methyl-pent-4-enoyl)-4-phenyl-imidazolidin-2-one

Guidance literature:: With sodium hexamethyldisilazane; at -78 ℃;
DOI:10.1016/S0040-4039(99)00438-4

Reference yield:

: 1027396-71-9
(4R,5S)-1,5-Dimethyl-3-((S)-2-methyl-pent-4-enoyl)-4-phenyl-imidazolidin-2-one

: 105-30-6,17092-41-0,17092-54-5,17092-42-1
(S)-2-methyl-1-pentanol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C

2: 85 percent / LiBH₄ / H₂O

With lithium borohydride; hydrogen; palladium on activated charcoal; In water;
DOI:10.1016/S0040-4039(99)00438-4

Reference yield:

: 1027396-71-9
(4R,5S)-1,5-Dimethyl-3-((S)-2-methyl-pent-4-enoyl)-4-phenyl-imidazolidin-2-one

: (E)-(2S,3S,6S)-3-(4-Methoxy-benzyloxy)-2,6-dimethyl-non-4-en-1-ol

Guidance literature:: Multi-step reaction with 9 steps

1: H₂ / Pd/C

2: 85 percent / LiBH₄ / H₂O

3: 1.) DMSO, (COCl)2; 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C; 2.) CH₂Cl₂, -78 deg C

5: DIBAL

6: 1.) DMSO, (COCl)2; 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C; 2.) CH₂Cl₂, -78 deg C

7: 67 percent / Bu₂BOTf, Et₃N

8: BF₃*Et₂O

9: LiBH₄ / H₂O

With lithium borohydride; oxalyl dichloride; di-n-butylboryl trifluoromethanesulfonate; boron trifluoride diethyl etherate; hydrogen; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; palladium on activated charcoal; In water;
DOI:10.1016/S0040-4039(99)00438-4