(2S,3S,4R)-(3,4-isopropylidenedioxy-1-(1'S,2'S,3'R,4'R,5'S)-2',3',4',5'-tetrabenzyloxycyclohexylaminooctadecan-2-yl)hexacosanamide

Base Information

Chemical Name:(2S,3S,4R)-(3,4-isopropylidenedioxy-1-(1'S,2'S,3'R,4'R,5'S)-2',3',4',5'-tetrabenzyloxycyclohexylaminooctadecan-2-yl)hexacosanamide
CAS No.:1198207-13-4
Molecular Formula:C₈₁H₁₂₈N₂O₇
Molecular Weight:1241.92
Hs Code.:

Synonyms:(2S,3S,4R)-(3,4-isopropylidenedioxy-1-(1'S,2'S,3'R,4'R,5'S)-2',3',4',5'-tetrabenzyloxycyclohexylaminooctadecan-2-yl)hexacosanamide

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Chemical Property of (2S,3S,4R)-(3,4-isopropylidenedioxy-1-(1'S,2'S,3'R,4'R,5'S)-2',3',4',5'-tetrabenzyloxycyclohexylaminooctadecan-2-yl)hexacosanamide

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Technology Process of (2S,3S,4R)-(3,4-isopropylidenedioxy-1-(1'S,2'S,3'R,4'R,5'S)-2',3',4',5'-tetrabenzyloxycyclohexylaminooctadecan-2-yl)hexacosanamide

There total 9 articles about (2S,3S,4R)-(3,4-isopropylidenedioxy-1-(1'S,2'S,3'R,4'R,5'S)-2',3',4',5'-tetrabenzyloxycyclohexylaminooctadecan-2-yl)hexacosanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 506-46-7
1-hexacosanoic acid

: 1198207-11-2
(S)-1-((4S,5R)-2, 2-dimethyl-5-tetradecyl-1,3-dioxolan-4-yl)-N₂-((1S,2S,3R,4R,5S)-2,3,4,5-tetrakis(benzyloxy)cyclohexyl)ethane-1,2-diamine

: 1198207-13-4
(2S,3S,4R)-(3,4-isopropylidenedioxy-1-(1'S,2'S,3'R,4'R,5'S)-2',3',4',5'-tetrabenzyloxycyclohexylaminooctadecan-2-yl)hexacosanamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; for 2h; Reflux;

Reference yield:

: 143396-09-2
(1R,2S,3R,4R,5S)-2,3,4,5-tetrakis(benzyloxy)cyclohexanol

: 1198207-13-4
(2S,3S,4R)-(3,4-isopropylidenedioxy-1-(1'S,2'S,3'R,4'R,5'S)-2',3',4',5'-tetrabenzyloxycyclohexylaminooctadecan-2-yl)hexacosanamide

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / tetrahydrofuran / 3 h / 20 °C

2: sodium azide / N,N-dimethyl-formamide / 12 h / 90 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C

4: acetonitrile / 3 h / Reflux

5: thiophenol; caesium carbonate / acetonitrile / 24 h / 20 °C

6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 2 h / Reflux

With lithium aluminium tetrahydride; sodium azide; caesium carbonate; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1198207-07-6
(1S,2S,3R,4R,5S)-2,3,4,5-tetrakis(benzyloxy)cyclohexanamine

: 1198207-13-4
(2S,3S,4R)-(3,4-isopropylidenedioxy-1-(1'S,2'S,3'R,4'R,5'S)-2',3',4',5'-tetrabenzyloxycyclohexylaminooctadecan-2-yl)hexacosanamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 3 h / Reflux

2: thiophenol; caesium carbonate / acetonitrile / 24 h / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 2 h / Reflux

With caesium carbonate; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; acetonitrile;