(Z)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone

Base Information

Chemical Name:(Z)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone
CAS No.:103869-89-2
Molecular Formula:C₁₄H₁₅ClN₄O
Molecular Weight:290.752
Hs Code.:

(Z)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<c><1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone

Synonyms:(Z)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone

Chemical Property:

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Technology Process of (Z)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone

There total 4 articles about (Z)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 1073-69-4
N-4-chlorophenylhydrazine

: 40345-59-3
4-oxo-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazole

: 103869-94-9
(E)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone

: 103869-89-2
(Z)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone

Guidance literature:: In ethanol; for 1h; Yields of byproduct given; Heating;
DOI:10.1002/hlca.19850680630

Reference yield:

: 103869-94-9
(E)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone

: 103869-89-2
(Z)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone

Guidance literature:: at 138 - 140 ℃; isomerization;
DOI:10.1002/hlca.19850680630

Reference yield:

: 1073-69-4
N-4-chlorophenylhydrazine

: 103869-89-2
(Z)-4,5,6,7-tetrahydro-6,6-dimethylbenzo<1,2,5>oxadiazol-4-one (p-chlorophenyl)hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / ethanol / 1 h / Heating

2: 138 - 140 °C / isomerization

In ethanol;
DOI:10.1002/hlca.19850680630