3-[{2'-(4-amino-5-sulfanyl-4H-1,2,4-triazol-3-yl)-(1,1'-biphenyl)-4-yl}methyl]-2,4-dioxo-1,3-thiazolidine

Base Information

Chemical Name:3-[{2'-(4-amino-5-sulfanyl-4H-1,2,4-triazol-3-yl)-(1,1'-biphenyl)-4-yl}methyl]-2,4-dioxo-1,3-thiazolidine
CAS No.:1338814-02-0
Molecular Formula:C₁₈H₁₅N₅O₂S₂
Molecular Weight:397.481
Hs Code.:

Synonyms:3-[{2'-(4-amino-5-sulfanyl-4H-1,2,4-triazol-3-yl)-(1,1'-biphenyl)-4-yl}methyl]-2,4-dioxo-1,3-thiazolidine

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Chemical Property of 3-[{2'-(4-amino-5-sulfanyl-4H-1,2,4-triazol-3-yl)-(1,1'-biphenyl)-4-yl}methyl]-2,4-dioxo-1,3-thiazolidine

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Technology Process of 3-[{2'-(4-amino-5-sulfanyl-4H-1,2,4-triazol-3-yl)-(1,1'-biphenyl)-4-yl}methyl]-2,4-dioxo-1,3-thiazolidine

There total 2 articles about 3-[{2'-(4-amino-5-sulfanyl-4H-1,2,4-triazol-3-yl)-(1,1'-biphenyl)-4-yl}methyl]-2,4-dioxo-1,3-thiazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1338814-01-9
4'-[(2,4-dioxo-1,3-thiazolidin-3-yl)methyl]-(1,1'-biphenyl)-2-carbohydrazide

: 1338814-02-0
3-[{2'-(4-amino-5-sulfanyl-4H-1,2,4-triazol-3-yl)-(1,1'-biphenyl)-4-yl}methyl]-2,4-dioxo-1,3-thiazolidine

Guidance literature:: carbon disulfide; 4'-[(2,4-dioxo-1,3-thiazolidin-3-yl)methyl]-(1,1'-biphenyl)-2-carbohydrazide; With potassium hydroxide; In ethanol; at 20 ℃; for 10h;

With hydrazine hydrate; In water; for 3h; Reflux;
DOI:10.1007/s12039-011-0101-8

Reference yield:

: 1338813-98-1
methyl 4'-[(2,4-dioxo-1,3-thiazolidin-3-yl)methyl]-(1,1'-biphenyl)-2-carboxylate

: 1338814-02-0
3-[{2'-(4-amino-5-sulfanyl-4H-1,2,4-triazol-3-yl)-(1,1'-biphenyl)-4-yl}methyl]-2,4-dioxo-1,3-thiazolidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazine hydrate / ethanol / 3 h / Reflux

2.1: potassium hydroxide / ethanol / 10 h / 20 °C

2.2: 3 h / Reflux

With hydrazine hydrate; potassium hydroxide; In ethanol;
DOI:10.1007/s12039-011-0101-8