4-(2-chlorophenyl)-8-(2,6-dichlorophenyI)-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)-1,7-naphthyridin-2-amine 7-oxide

Base Information

Chemical Name:4-(2-chlorophenyl)-8-(2,6-dichlorophenyI)-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)-1,7-naphthyridin-2-amine 7-oxide
CAS No.:1344669-02-8
Molecular Formula:C₃₀H₃₁Cl₃N₄O
Molecular Weight:569.961
Hs Code.:

Synonyms:4-(2-chlorophenyl)-8-(2,6-dichlorophenyI)-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)-1,7-naphthyridin-2-amine 7-oxide

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Chemical Property of 4-(2-chlorophenyl)-8-(2,6-dichlorophenyI)-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)-1,7-naphthyridin-2-amine 7-oxide

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Technology Process of 4-(2-chlorophenyl)-8-(2,6-dichlorophenyI)-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)-1,7-naphthyridin-2-amine 7-oxide

There total 6 articles about 4-(2-chlorophenyl)-8-(2,6-dichlorophenyI)-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)-1,7-naphthyridin-2-amine 7-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

: 40327-96-6
4-amino-1,2,2,6,6-pentamethylpiperidine

: 1075255-34-3
2-chloro-4-(2-chlorophenyl)-8-(2,6-dichlorophenyl)-1,7-naphthyridine 7-oxide

: 1344669-02-8
4-(2-chlorophenyl)-8-(2,6-dichlorophenyI)-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)-1,7-naphthyridin-2-amine 7-oxide

Guidance literature:: In 2-ethoxy-ethanol; for 3h; Sealed tube; Heating;
DOI:10.1021/jm200975u

Reference yield:

: 1075255-04-7
4-(2-chlorophenyl)-8-(2,6-dichlorophenyl)-1,7-naphthyridin-2(1H)-one

: 1344669-02-8
4-(2-chlorophenyl)-8-(2,6-dichlorophenyI)-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)-1,7-naphthyridin-2-amine 7-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: dihydrogen peroxide; acetic acid / water / 16 h / 95 °C / Sealed tube

2: trichlorophosphate / 2 h / 110 °C / Sealed tube

3: 2-ethoxy-ethanol / 3 h / Sealed tube; Heating

With dihydrogen peroxide; acetic acid; trichlorophosphate; In 2-ethoxy-ethanol; water;
DOI:10.1021/jm200975u

Reference yield:

: 1075255-05-8
4-(2-chlorophenyl)-8-(2,6-dichlorophenyl)-1,7-naphthyridin-2(1H)-one 7-oxide

: 1344669-02-8
4-(2-chlorophenyl)-8-(2,6-dichlorophenyI)-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)-1,7-naphthyridin-2-amine 7-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 2 h / 110 °C / Sealed tube

2: 2-ethoxy-ethanol / 3 h / Sealed tube; Heating

With trichlorophosphate; In 2-ethoxy-ethanol;
DOI:10.1021/jm200975u