C₆₀H₇₄O₁₆

Base Information

Chemical Name:C₆₀H₇₄O₁₆
CAS No.:318261-96-0
Molecular Formula:C₆₀H₇₄O₁₆
Molecular Weight:1051.24
Hs Code.:

C<sub>60</sub>H<sub>74</sub>O<sub>16</sub>

Synonyms:C₆₀H₇₄O₁₆

Suppliers and Price of C₆₀H₇₄O₁₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₀H₇₄O₁₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₀H₇₄O₁₆

There total 15 articles about C₆₀H₇₄O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 318261-40-4
(3,5-dibromo-phenyl)-pyrrolidin-1-yl-diazene

: 318261-96-0
C₆₀H₇₄O₁₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-BuLi; B(OMe)3 / diethyl ether / 2 h

1.2: CH₃CO₃H / diethyl ether / 1 h / 0 °C

2.1: DEAD; PPh₃ / tetrahydrofuran

3.1: 80 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / 18 h / 80 °C

4.1: 76 percent / CH₃I / 12 h / 110 °C

5.1: 79 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / 70 °C

6.1: TBAF; H₂O / tetrahydrofuran / 0.01 h / 20 °C

7.1: 87 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / acetonitrile / 70 °C

8.1: TBAF; H₂O / tetrahydrofuran / 0.01 h / 20 °C

With copper(l) iodide; n-butyllithium; Trimethyl borate; tetrabutyl ammonium fluoride; water; triethylamine; triphenylphosphine; diethylazodicarboxylate; methyl iodide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; diethyl ether; acetonitrile; 2.1: Mitsunobu coupling / 3.1: Sonogashira coupling;
DOI:10.1021/ja002129e

Reference yield:

: 3-bromo-5-(pyrrolidin-1-ylazo)-phenol

: 318261-96-0
C₆₀H₇₄O₁₆

Guidance literature:: Multi-step reaction with 7 steps

1: DEAD; PPh₃ / tetrahydrofuran

2: 80 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / 18 h / 80 °C

3: 76 percent / CH₃I / 12 h / 110 °C

4: 79 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / 70 °C

5: TBAF; H₂O / tetrahydrofuran / 0.01 h / 20 °C

6: 87 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / acetonitrile / 70 °C

7: TBAF; H₂O / tetrahydrofuran / 0.01 h / 20 °C

With copper(l) iodide; tetrabutyl ammonium fluoride; water; triethylamine; triphenylphosphine; diethylazodicarboxylate; methyl iodide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; acetonitrile; 1: Mitsunobu coupling / 2: Sonogashira coupling;
DOI:10.1021/ja002129e

Reference yield:

: (3-bromo-5-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-phenyl)-pyrrolidin-1-yl-diazene

: 318261-96-0
C₆₀H₇₄O₁₆

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / 18 h / 80 °C

2: 76 percent / CH₃I / 12 h / 110 °C

3: 79 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / 70 °C

4: TBAF; H₂O / tetrahydrofuran / 0.01 h / 20 °C

5: 87 percent / CuI; PPh₃; NEt₃ / Pd₂(dba)3 / acetonitrile / 70 °C

6: TBAF; H₂O / tetrahydrofuran / 0.01 h / 20 °C

With copper(l) iodide; tetrabutyl ammonium fluoride; water; triethylamine; triphenylphosphine; methyl iodide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; acetonitrile; 1: Sonogashira coupling;
DOI:10.1021/ja002129e