trans-4-azobenzene

Base Information

Chemical Name:trans-4-azobenzene
CAS No.:220290-77-7
Molecular Formula:C₃₆H₂₇N₃
Molecular Weight:501.63
Hs Code.:

trans-4-<di(biphenyl-4-yl)amino>azobenzene

Synonyms:trans-4-azobenzene

Suppliers and Price of trans-4-azobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-4-azobenzene

Chemical Property:

Purity/Quality:

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Technology Process of trans-4-azobenzene

There total 5 articles about trans-4-azobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1591-31-7
4-iodo-biphenyl

: 60-09-3
aniline yellow

: 220290-77-7
trans-4-azobenzene

Guidance literature:: With potassium hydroxide; copper; In decalin; at 150 ℃; for 8h;
DOI:10.1039/a806802j

Reference yield:

: bis-(4-bromo-phenyl)-(4-phenylazo-phenyl)-amine

: 98-80-6
phenylboronic acid

: 220290-77-7
trans-4-azobenzene

Guidance literature:: With sodium carbonate; In toluene; at 80 ℃;
DOI:10.1021/ja038207q

Reference yield:

: 603-34-9
N,N-diphenylaminobenzene

: 220290-77-7
trans-4-azobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: NaDBS / CH₂Cl₂; H₂O / 20 °C

2: NBS / CH₂Cl₂ / 4 h / Heating

3: Na₂CO₃ / toluene / 80 °C

With N-Bromosuccinimide; sodium carbonate; In dichloromethane; water; toluene;
DOI:10.1021/ja038207q