(S)-2-(((benzyloxy)carbonyl)amino)[1,2,3-¹³C₃, 2,3,3,3-²H_4]propanoic acid

Base Information

Chemical Name:(S)-2-(((benzyloxy)carbonyl)amino)[1,2,3-¹³C₃, 2,3,3,3-²H_4]propanoic acid
CAS No.:1467710-09-3
Molecular Formula:C₁₁H₁₃NO₄
Molecular Weight:230.164
Hs Code.:

(S)-2-(((benzyloxy)carbonyl)amino)[1,2,3-<sup>13</sup>C<sub>3</sub>, 2,3,3,3-<sup>2</sup>H<sub>4]</sub>propanoic acid

Synonyms:(S)-2-(((benzyloxy)carbonyl)amino)[1,2,3-¹³C₃, 2,3,3,3-²H_4]propanoic acid

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Chemical Property of (S)-2-(((benzyloxy)carbonyl)amino)[1,2,3-¹³C₃, 2,3,3,3-²H_4]propanoic acid

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Technology Process of (S)-2-(((benzyloxy)carbonyl)amino)[1,2,3-¹³C₃, 2,3,3,3-²H_4]propanoic acid

There total 1 articles about (S)-2-(((benzyloxy)carbonyl)amino)[1,2,3-¹³C₃, 2,3,3,3-²H_4]propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1217450-97-9,100108-77-8,244237-64-7,53795-94-1,65163-26-0,70753-82-1
(S)-2-amino[1,2,3-¹³C₃, 2,3,3,3-²H_4]propanoic acid

: 501-53-1,94274-21-2
benzyl chloroformate

: 1467710-09-3
(S)-2-(((benzyloxy)carbonyl)amino)[1,2,3-¹³C₃, 2,3,3,3-²H_4]propanoic acid

Guidance literature:: With sodium hydroxide; In water; toluene; at 5 - 20 ℃; for 0.5h; Cooling with ice;
DOI:10.1002/jlcr.3078

Reference yield: 98.0%

: 5681-36-7,3026-45-7
1,2-dipalmitoyl-sn-glycero-3-phospoethanolamine

: 1467710-09-3
(S)-2-(((benzyloxy)carbonyl)amino)[1,2,3-¹³C₃, 2,3,3,3-²H_4]propanoic acid

: 3-(((2-((S)-2-(((benzyloxy)carbonyl)amino)[1,2,3-¹³C₃, 2,3,3,3-²H_4]propanamido)ethoxy)(hydroxy)phosphoryl)oxy)propane-1,2-diyl dipalmitate

Guidance literature:: (S)-2-(((benzyloxy)carbonyl)amino)[1,2,3-¹³C₃, 2,3,3,3-²H_4]propanoic acid; With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 5h; Cooling with ice;

1,2-dipalmitoyl-sn-glycero-3-phospoethanolamine; With triethylamine; In methanol; chloroform; N,N-dimethyl-formamide; Inert atmosphere;
DOI:10.1002/jlcr.3078