tert-butyl N-[({6-[3-(methylsulfonyl)phenyl]-1,3-benzothiazol-2-yl}amino)carbonyl]-β-alaninate

Base Information

Chemical Name:tert-butyl N-[({6-[3-(methylsulfonyl)phenyl]-1,3-benzothiazol-2-yl}amino)carbonyl]-β-alaninate
CAS No.:1192831-79-0
Molecular Formula:C₂₂H₂₅N₃O₅S₂
Molecular Weight:475.59
Hs Code.:

Synonyms:tert-butyl N-[({6-[3-(methylsulfonyl)phenyl]-1,3-benzothiazol-2-yl}amino)carbonyl]-β-alaninate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl N-[({6-[3-(methylsulfonyl)phenyl]-1,3-benzothiazol-2-yl}amino)carbonyl]-β-alaninate

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Technology Process of tert-butyl N-[({6-[3-(methylsulfonyl)phenyl]-1,3-benzothiazol-2-yl}amino)carbonyl]-β-alaninate

There total 2 articles about tert-butyl N-[({6-[3-(methylsulfonyl)phenyl]-1,3-benzothiazol-2-yl}amino)carbonyl]-β-alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1192832-20-4
N-{6-[3-(methylsulfonyl)phenyl]-1,3-benzothiazol-2-yl}-1H-imidazole-1-carboxamide

: 58620-93-2
tert-butyl 3-aminopropanoate hydrochloride

: 1192831-79-0
tert-butyl N-[({6-[3-(methylsulfonyl)phenyl]-1,3-benzothiazol-2-yl}amino)carbonyl]-β-alaninate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 100 ℃; for 15h;

Reference yield:

: 1192831-43-8
6-[3-(methylsulfonyl)phenyl]-1,3-benzothiazol-2-amine

: 1192831-79-0
tert-butyl N-[({6-[3-(methylsulfonyl)phenyl]-1,3-benzothiazol-2-yl}amino)carbonyl]-β-alaninate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 15 h / 20 °C

2: triethylamine / N,N-dimethyl-formamide / 15 h / 100 °C

With triethylamine; In N,N-dimethyl-formamide; acetonitrile;