(S)-S-phenyl 2-(3-(2-azidoacetamido)propanamido)-3-phenylpropanethioate

Base Information

Chemical Name:(S)-S-phenyl 2-(3-(2-azidoacetamido)propanamido)-3-phenylpropanethioate
CAS No.:1401355-50-7
Molecular Formula:C₂₀H₂₁N₅O₃S
Molecular Weight:411.484
Hs Code.:

Synonyms:(S)-S-phenyl 2-(3-(2-azidoacetamido)propanamido)-3-phenylpropanethioate

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Chemical Property of (S)-S-phenyl 2-(3-(2-azidoacetamido)propanamido)-3-phenylpropanethioate

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Technology Process of (S)-S-phenyl 2-(3-(2-azidoacetamido)propanamido)-3-phenylpropanethioate

There total 4 articles about (S)-S-phenyl 2-(3-(2-azidoacetamido)propanamido)-3-phenylpropanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1401355-49-4
(S)-2-(3-(2-azidoacetamido)propanamido)-3-phenylpropanoic acid

: 108-98-5
thiophenol

: 1401355-50-7
(S)-S-phenyl 2-(3-(2-azidoacetamido)propanamido)-3-phenylpropanethioate

Guidance literature:: (S)-2-(3-(2-azidoacetamido)propanamido)-3-phenylpropanoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at 0 ℃; for 0.0833333h; Inert atmosphere;

thiophenol; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c2ob25996f

Reference yield:

: 908572-06-5
(S)-2-(3-aminopropanamido)-3-phenylpropanoic acid hydrochloride

: 1401355-50-7
(S)-S-phenyl 2-(3-(2-azidoacetamido)propanamido)-3-phenylpropanethioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 2.5 h / 0 °C / Reflux; Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 72 h / 80 °C / Inert atmosphere

3.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

3.2: 24 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; sodium azide; isobutyl chloroformate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c2ob25996f

Reference yield:

: 1401355-48-3
(S)-2-(3-(2-chloroacetamido)propanamido)-3-phenylpropanoic acid

: 1401355-50-7
(S)-S-phenyl 2-(3-(2-azidoacetamido)propanamido)-3-phenylpropanethioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium azide / N,N-dimethyl-formamide / 72 h / 80 °C / Inert atmosphere

2.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

2.2: 24 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; sodium azide; isobutyl chloroformate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c2ob25996f