(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2R,3E)-2-hydroxy-3-octadecenoate

Base Information

Chemical Name:(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2R,3E)-2-hydroxy-3-octadecenoate
CAS No.:150178-55-5
Molecular Formula:C₃₄H₅₆O₃
Molecular Weight:512.817
Hs Code.:

Synonyms:(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2R,3E)-2-hydroxy-3-octadecenoate

Suppliers and Price of (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2R,3E)-2-hydroxy-3-octadecenoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2R,3E)-2-hydroxy-3-octadecenoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2R,3E)-2-hydroxy-3-octadecenoate

There total 3 articles about (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2R,3E)-2-hydroxy-3-octadecenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 150178-57-7
(E)-2-Oxo-octadec-3-enoic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 150178-55-5
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2R,3E)-2-hydroxy-3-octadecenoate

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; L-Selectride; Yield given. Multistep reaction; 1.) Et₂O, -78 deg C, 1 h, 2.) MeOH, -78 deg C to r.t., 1 h;
DOI:10.1021/jo00068a056

Reference yield:

: 629-76-5
pentadecanol

: 150178-55-5
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2R,3E)-2-hydroxy-3-octadecenoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) PCC, 2.) H⁽¹⁺⁾

2: 1.) BF₃*OEt₂, 2.) SiO₂ / 1.) CH₂Cl₂, -78 to 0 deg C, 2.) C₆H₆, reflux

4: 1.) L-selectride, 2.) 10percent aq. NaOH, 30percent aq. H₂O₂ / 1.) Et₂O, -78 deg C, 1 h, 2.) MeOH, -78 deg C to r.t., 1 h

With sodium hydroxide; boron trifluoride diethyl etherate; dihydrogen peroxide; silica gel; hydrogen cation; L-Selectride; pyridinium chlorochromate;
DOI:10.1021/jo00068a056

Reference yield:

: 1027208-67-8
ethyl (E)-2-oxo-3-octadecenoate

: 150178-55-5
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2R,3E)-2-hydroxy-3-octadecenoate

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) L-selectride, 2.) 10percent aq. NaOH, 30percent aq. H₂O₂ / 1.) Et₂O, -78 deg C, 1 h, 2.) MeOH, -78 deg C to r.t., 1 h

With sodium hydroxide; dihydrogen peroxide; L-Selectride;
DOI:10.1021/jo00068a056