2-methyl-propane-2-sulfinic acid [(Z)-3-oxo-1-(2,4,5-trifluorobenzyl)-3-(3-trifluoromethyl-5,6-dihydro-8H-[1,2,4]triazolo[4,3-a]pyrazin-7-yl)-propenyl]amide

Base Information

• Chemical Name: 2-methyl-propane-2-sulfinic acid [(Z)-3-oxo-1-(2,4,5-trifluorobenzyl)-3-(3-trifluoromethyl-5,6-dihydro-8H-[1,2,4]triazolo[4,3-a]pyrazin-7-yl)-propenyl]amide
• CAS No.: 1349649-78-0
• Molecular Formula: C₂₀H₂₁F₆N₅O₂S
• Molecular Weight: 509.475

Synonyms:2-methyl-propane-2-sulfinic acid [(Z)-3-oxo-1-(2,4,5-trifluorobenzyl)-3-(3-trifluoromethyl-5,6-dihydro-8H-[1,2,4]triazolo[4,3-a]pyrazin-7-yl)-propenyl]amide

Chemical Property of 2-methyl-propane-2-sulfinic acid [(Z)-3-oxo-1-(2,4,5-trifluorobenzyl)-3-(3-trifluoromethyl-5,6-dihydro-8H-[1,2,4]triazolo[4,3-a]pyrazin-7-yl)-propenyl]amide

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Technology Process of 2-methyl-propane-2-sulfinic acid [(Z)-3-oxo-1-(2,4,5-trifluorobenzyl)-3-(3-trifluoromethyl-5,6-dihydro-8H-[1,2,4]triazolo[4,3-a]pyrazin-7-yl)-propenyl]amide

There total 1 articles about 2-methyl-propane-2-sulfinic acid [(Z)-3-oxo-1-(2,4,5-trifluorobenzyl)-3-(3-trifluoromethyl-5,6-dihydro-8H-[1,2,4]triazolo[4,3-a]pyrazin-7-yl)-propenyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

S-tert-butylsulfinimide (146374-27-8) + 1-(3-(trifluoromethyl)-5,6-dihydro-[1,2,4]triazolo[4,3-a]pyrazin-7(8H)-yl)-4-(2,4,5-trifluorophenyl)butane-1,3-dione (764667-65-4) → 2-methyl-propane-2-sulfinic acid [(Z)-3-oxo-1-(2,4,5-trifluorobenzyl)-3-(3-trifluoromethyl-5,6-dihydro-8H-[1,2,4]triazolo[4,3-a]pyrazin-7-yl)-propenyl]amide (1349649-78-0)

Guidance literature:

toluene-4-sulfonic acid; In toluene; Reflux;

Reference yield:

2-methyl-propane-2-sulfinic acid [(Z)-3-oxo-1-(2,4,5-trifluorobenzyl)-3-(3-trifluoromethyl-5,6-dihydro-8H-[1,2,4]triazolo[4,3-a]pyrazin-7-yl)-propenyl]amide (1349649-78-0) → 2-methyl-propane-2-sulfinic acid [3-oxo-1-(2,4,5-trifluorobenzyl)-3-(3-trifluoromethyl-5,6-dihydro-8H-[1,2,4]triazolo[4,3-a]pyrazin-7-yl)-propyl]amide (1349649-80-4)

Guidance literature:

With sodium tetrahydroborate; acetic acid; In dichloromethane; for 0.5h;

upstream raw materials:

S-tert-butylsulfinimide

1-(3-(trifluoromethyl)-5,6-dihydro-[1,2,4]triazolo[4,3-a]pyrazin-7(8H)-yl)-4-(2,4,5-trifluorophenyl)butane-1,3-dione

Downstream raw materials:

2-methyl-propane-2-sulfinic acid [3-oxo-1-(2,4,5-trifluorobenzyl)-3-(3-trifluoromethyl-5,6-dihydro-8H-[1,2,4]triazolo[4,3-a]pyrazin-7-yl)-propyl]amide

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