4-Methoxycarbonyloxybenzoicacid

Base Information

• Chemical Name: 4-Methoxycarbonyloxybenzoicacid
• CAS No.: 14180-11-1
• Molecular Formula: C9H8 O5
• Molecular Weight: 196.16
• Hs Code.: 2918990090
• Mol file: 14180-11-1.mol

Synonyms:Carbonicacid, methyl ester, ester with p-hydroxybenzoic acid (7CI,8CI);4-(Methoxycarbonyloxy)benzoic acid

Chemical Property of 4-Methoxycarbonyloxybenzoicacid

Chemical Property:

• Melting Point: 169-171 °C(Solv: ethanol (64-17-5))
• Boiling Point: 351.3±34.0 °C(Predicted)
• PKA: 4.05±0.10(Predicted)
• PSA: 72.83000
• Density: 1.343±0.06 g/cm3(Predicted)
• LogP: 1.53000

Purity/Quality:

99% ^*data from raw suppliers

4-[(Methoxycarbonyl)oxy]benzoic acid 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Methoxycarbonyloxybenzoicacid

There total 2 articles about 4-Methoxycarbonyloxybenzoicacid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methyl chloroformate (79-22-1) + 4-hydroxy-benzoic acid (99-96-7) → 4-(methoxycarbonyloxy)benzoic acid (14180-11-1)

Guidance literature:

With sodium hydroxide; at 20 ℃;

DOI:10.1016/S0957-4166(99)00416-4

Reference yield:

furan-2,3,5(4H)-trione pyridine (1:1) + methyl chloroformate (79-22-1) + 4-hydroxy-benzoic acid (99-96-7) → 4-(methoxycarbonyloxy)benzoic acid (14180-11-1)

Guidance literature:

Reference yield: 100.0%

4-(methoxycarbonyloxy)benzoic acid (14180-11-1) → 4-methoxycarbonyloxybenzoyl chloride (78152-12-2)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide;

DOI:10.1016/j.tet.2010.03.025

upstream raw materials:

methyl chloroformate

4-hydroxy-benzoic acid

Downstream raw materials:

4-methoxycarbonyloxy-benzoic acid anilide

4-methoxycarbonyloxybenzoyl chloride

4-Methoxycarbonyloxy-benzoic acid heptyl ester

4-Methoxycarbonyloxy-benzoic acid nonyl ester

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