benzyl ((S)-1-(((S)-1-hydroxypropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

Base Information

Chemical Name:benzyl ((S)-1-(((S)-1-hydroxypropan-2-yl)amino)-1-oxopropan-2-yl)carbamate
CAS No.:129221-00-7
Molecular Formula:C₁₄H₂₀N₂O₄
Molecular Weight:280.324
Hs Code.:

Synonyms:benzyl ((S)-1-(((S)-1-hydroxypropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

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Chemical Property of benzyl ((S)-1-(((S)-1-hydroxypropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

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Technology Process of benzyl ((S)-1-(((S)-1-hydroxypropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

There total 4 articles about benzyl ((S)-1-(((S)-1-hydroxypropan-2-yl)amino)-1-oxopropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 2483-51-4
N-[(benzyloxy)carbonyl]-L-alanyl-L-alanine methyl ester

: 129221-00-7
benzyl ((S)-1-(((S)-1-hydroxypropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; water; at 0 - 25 ℃; for 18h;
DOI:10.1016/j.chempr.2021.08.011

Reference yield:

: 1072841-09-8
C₂₀H₂₁N₅O₄

: 129221-00-7
benzyl ((S)-1-(((S)-1-hydroxypropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃;
DOI:10.3184/030823407X272985

Reference yield:

: 16012-70-7
benzyloxycarbonyl-L-alanyl-L-alanine

: 129221-00-7
benzyl ((S)-1-(((S)-1-hydroxypropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

Guidance literature:: With pyridine; methanol; sodium tetrahydroborate; trifluoro-[1,3,5]triazine; Yield given. Multistep reaction; 1.) CH₂Cl₂, -20 to -010 deg C, 1 h, 2.) room temperature, 10-15 min;
DOI:10.1021/jo9520699