3-Chloro-4,5-difluoro-1,2-diaminobenzene

Base Information

Chemical Name:3-Chloro-4,5-difluoro-1,2-diaminobenzene
CAS No.:153505-34-1
Molecular Formula:C₆H₅ClF₂N₂
Molecular Weight:178.569
Hs Code.:
DSSTox Substance ID:DTXSID601276703

Synonyms:153505-34-1;3-Chloro-4,5-difluoro-1,2-diaminobenzene;3-chloro-4,5-difluorobenzene-1,2-diamine;1,2-Benzenediamine, 3-chloro-4,5-difluoro-;SCHEMBL4706186;CUEKPFMYASVWIC-UHFFFAOYSA-N;DTXSID601276703;3-Chloro-4,5-difluoro-1,2-benzenediamine

Suppliers and Price of 3-Chloro-4,5-difluoro-1,2-diaminobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-Chloro-4,5-difluoro-1,2-diaminobenzene

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:178.0109322
Heavy Atom Count:11
Complexity:147

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=C(C(=C(C(=C1F)F)Cl)N)N

Technology Process of 3-Chloro-4,5-difluoro-1,2-diaminobenzene

There total 3 articles about 3-Chloro-4,5-difluoro-1,2-diaminobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: SnCl₂ 2H₂ O

: 112062-56-3
2-chloro-3,4-difluoro-6-nitroaniline

: 153505-34-1
3-chloro-4,5-difluoro-1,2-diaminobenzene

Guidance literature:: With sodium hydrogencarbonate; In ethanol; ethyl acetate;

Reference yield:

: 112062-56-3
2-chloro-3,4-difluoro-6-nitroaniline

: 153505-34-1
3-chloro-4,5-difluoro-1,2-diaminobenzene

Guidance literature:: With tin(ll) chloride; In ethanol; ethyl acetate; at 70 ℃; for 0.583333h;
DOI:10.1021/jm00022a003

Reference yield:

: 78056-39-0
4,5-difluoro-2-nitroaniline

: 153505-34-1
3-chloro-4,5-difluoro-1,2-diaminobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: NCS / dimethylformamide / 120 h / Ambient temperature

2: SnCl₂*H₂O / ethyl acetate; ethanol / 0.58 h / 70 °C

With N-chloro-succinimide; tin(ll) chloride; In ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00022a003