4'-isopropoxy-2-methoxy-2'-methyl-6-nitrobiphenyl

Base Information

Chemical Name:4'-isopropoxy-2-methoxy-2'-methyl-6-nitrobiphenyl
CAS No.:111220-38-3
Molecular Formula:C₁₇H₁₉NO₄
Molecular Weight:301.342
Hs Code.:

Synonyms:4'-isopropoxy-2-methoxy-2'-methyl-6-nitrobiphenyl

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Chemical Property of 4'-isopropoxy-2-methoxy-2'-methyl-6-nitrobiphenyl

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Technology Process of 4'-isopropoxy-2-methoxy-2'-methyl-6-nitrobiphenyl

There total 1 articles about 4'-isopropoxy-2-methoxy-2'-methyl-6-nitrobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19177-04-9
1-isopropoxy-3-methylbenzene

: 111220-38-3
4'-isopropoxy-2-methoxy-2'-methyl-6-nitrobiphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: 52 g / iodine/periodic acid / acetic acid; H₂O; H₂SO₄ / 6 h

2: 128.6 g / copper(I) t-butoxide / 1,2-dimethoxy-ethane; pyridine / 15 h / 75 - 80 °C

3: 110 g / hexamethylphosphoric acid triamide / 24 h

With iodine; copper (I) tert-butoxide; periodic acid; In pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; sulfuric acid; water; acetic acid;

Reference yield:

: 111220-38-3
4'-isopropoxy-2-methoxy-2'-methyl-6-nitrobiphenyl

: 111221-12-6
3,8-dimethoxy-4,7-bis-(4-isopropyl-2-methylphenyl)benzocinnoline

Guidance literature:: Multi-step reaction with 4 steps

1: 14.45 g / iodine/periodic acid dihydrate / H₂O; acetic acid; H₂SO₄ / 36 h / 80 °C

2: 6.3 g / copper(II)trifluoromethanesulphonate/copper powder, aq NH₃ / acetone; acetonitrile; dimethylsulfoxide / 1.) 0 deg C, 8 h; 2.) 5 deg C, 12 h

3: 3.6 g / zinc-copper couple / H₂O; acetic acid / 42 h / 125 °C

4: 1.) hydrochloric acid/sodium nitrite, 2.) urea, mercuric iodide/sodium iodide / 1.) dimethylformamide/water, -1 deg C, 3.5 h; 2.) dimethylformamide/water, 0 to 5 deg C, 3 h, dimethylsulfoxide, 120 to 125 deg C, 22 h

With hydrogenchloride; ammonium hydroxide; zinc copper; iodine; copper(II) bis(trifluoromethanesulfonate); copper; periodic acid; urea; sodium iodide; mercury(II) iodide; sodium nitrite; In sulfuric acid; water; acetic acid; dimethyl sulfoxide; acetone; acetonitrile;

Reference yield:

: 111220-38-3
4'-isopropoxy-2-methoxy-2'-methyl-6-nitrobiphenyl

: 111220-49-6
4,4'''-di-isopropoxy-4'',6'-dimethoxy-2,2'''-dimethyl-m-quaterphenyl-2',2''-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: 14.45 g / iodine/periodic acid dihydrate / H₂O; acetic acid; H₂SO₄ / 36 h / 80 °C

2: 6.3 g / copper(II)trifluoromethanesulphonate/copper powder, aq NH₃ / acetone; acetonitrile; dimethylsulfoxide / 1.) 0 deg C, 8 h; 2.) 5 deg C, 12 h

3: 3.6 g / zinc-copper couple / H₂O; acetic acid / 42 h / 125 °C

With ammonium hydroxide; zinc copper; iodine; copper(II) bis(trifluoromethanesulfonate); copper; periodic acid; In sulfuric acid; water; acetic acid; dimethyl sulfoxide; acetone; acetonitrile;